PMID- 28958527
OWN - NLM
STAT- MEDLINE
DCOM- 20171108
LR  - 20181202
IS  - 1873-7072 (Electronic)
IS  - 0308-8146 (Linking)
VI  - 241
DP  - 2018 Feb 15
TI  - Simultaneous determination of 124 pesticide residues in Chinese liquor and 
      liquor-making raw materials (sorghum and rice hull) by rapid Multi-plug 
      Filtration Cleanup and gas chromatography-tandem mass spectrometry.
PG  - 258-267
LID - S0308-8146(17)31436-X [pii]
LID - 10.1016/j.foodchem.2017.08.103 [doi]
AB  - A multi-residue method was developed for the determination of 124 pesticide 
      residues in Chinese liquor and liquor-making raw materials (sorghum and rice 
      hull) by rapid Multi-plug Filtration Cleanup (m-PFC) and GC-MS/MS detection. 
      Different combination and proportion sets of sorbents were initially optimized 
      for each matrix with adispersive solid-phase extraction (d-SPE) procedure. 
      Satisfactory linearity was obtained for the 124 pesticides with regression 
      coefficients (R(2)) greater than 0.9901. Mean recoveries of 121 pesticides were 
      in the range of 71-121% with Relative Standard Deviations (RSDs) lower than 16.8% 
      except cyprodinil, diflufenican and prothioconazole. The Limit of Quantification 
      (LOQs) was in the range of 1.0x10(-4)-5.0x10(-3)mgkg(-1) and the Limit of 
      Detection (LODs) ranged from 3.0x10(-5) to 1.5x10(-3)mgkg(-1) for the 124 
      pesticides in the matrices. It is demonstrated the m-PFC procedure is superior to 
      the d-SPE method and it could be used to routinely monitor of pesticide residues 
      in market samples.
CI  - Copyright (c) 2017 Elsevier Ltd. All rights reserved.
FAU - Han, Yongtao
AU  - Han Y
AD  - Department of Applied Chemistry, College of Science, China Agricultural 
      University, Beijing 100193, PR China.
FAU - Song, Le
AU  - Song L
AD  - Department of Applied Chemistry, College of Science, China Agricultural 
      University, Beijing 100193, PR China.
FAU - Liu, Shaowen
AU  - Liu S
AD  - Department of Applied Chemistry, College of Science, China Agricultural 
      University, Beijing 100193, PR China.
FAU - Zou, Nan
AU  - Zou N
AD  - Department of Applied Chemistry, College of Science, China Agricultural 
      University, Beijing 100193, PR China.
FAU - Li, Yanjie
AU  - Li Y
AD  - Department of Applied Chemistry, College of Science, China Agricultural 
      University, Beijing 100193, PR China.
FAU - Qin, Yuhong
AU  - Qin Y
AD  - Department of Applied Chemistry, College of Science, China Agricultural 
      University, Beijing 100193, PR China.
FAU - Li, Xuesheng
AU  - Li X
AD  - Institute of Pesticide and Environmental Toxicology, Guangxi University, Nanning 
      530005, PR China.
FAU - Pan, Canping
AU  - Pan C
AD  - Department of Applied Chemistry, College of Science, China Agricultural 
      University, Beijing 100193, PR China; Institute of Pesticide and Environmental 
      Toxicology, Guangxi University, Nanning 530005, PR China. Electronic address: 
      canpingp@cau.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20170901
PL  - England
TA  - Food Chem
JT  - Food chemistry
JID - 7702639
RN  - 0 (Pesticide Residues)
SB  - IM
MH  - Alcoholic Beverages/*analysis
MH  - Gas Chromatography-Mass Spectrometry
MH  - *Oryza
MH  - Pesticide Residues/*analysis
MH  - *Sorghum
MH  - Tandem Mass Spectrometry
OTO - NOTNLM
OT  - GC-MS/MS
OT  - Multi-residue
OT  - Pesticide residues
OT  - d-SPE
OT  - m-PFC
EDAT- 2017/09/30 06:00
MHDA- 2017/11/09 06:00
CRDT- 2017/09/30 06:00
PHST- 2016/03/16 00:00 [received]
PHST- 2017/05/18 00:00 [revised]
PHST- 2017/08/29 00:00 [accepted]
PHST- 2017/09/30 06:00 [entrez]
PHST- 2017/09/30 06:00 [pubmed]
PHST- 2017/11/09 06:00 [medline]
AID - S0308-8146(17)31436-X [pii]
AID - 10.1016/j.foodchem.2017.08.103 [doi]
PST - ppublish
SO  - Food Chem. 2018 Feb 15;241:258-267. doi: 10.1016/j.foodchem.2017.08.103. Epub 
      2017 Sep 1.