PMID- 29048807
OWN - NLM
STAT- MEDLINE
DCOM- 20181109
LR  - 20181109
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 35
IP  - 10
DP  - 2017 Oct 8
TI  - [Rapid determination of 10 volatile N-nitrosamines in sour meats by modified 
      QuEChERS and gas chromatography- triple quadrupole mass spectrometry].
PG  - 1086-1093
LID - 10.3724/SP.J.1123.2017.06006 [doi]
AB  - A rapid gas chromatography-triple quadrupole mass spectrometry (GC-MS/MS) method 
      with modified QuEChERS method was developed for the determination of 10 volatile 
      N-nitrosamines in sour meats. The samples were extracted with acetonitrile and 
      eliminated the fat with n-hexane. The extracts in acetonitrile layer were 
      purified by octadecyl silane (C18) and primary secondary amine (PSA) sorbents. 
      The N-nitrosamines were determined on a DB-WAX column (30 mx0.25 mmx0.25 mum) by 
      GC-MS/MS in selected reaction monitoring (SRM) mode. The external standard method 
      was used to quantify the N-nitrosamines. The correlation coefficients (r) of the 
      standard calibration curves were greater than 0.99 in the range of 1-100 mug/L. 
      The average recoveries ranged from 79.8% to 115.3% with the relative standard 
      deviations (RSDs) from 0.6% to 22.9% (n=6). The limits of detection (LODs, S/N=3) 
      and limits of quantification (LOQs, S/N=10) were 0.04-0.3 mug/kg and 0.1-1 mug/kg, 
      respectively. The developed method is simple, rapid, sensitive and efficient for 
      the screening of the N-nitrosamines in sour meats.
FAU - Zhao, Zhuang
AU  - Zhao Z
AD  - Guangxi Institute for Food and Drug Control, Nanning 530021, China.
FAU - Xu, Yangbiao
AU  - Xu Y
AD  - Guangxi Institute for Food and Drug Control, Nanning 530021, China.
FAU - Liu, Xianghong
AU  - Liu X
AD  - Guangxi Institute for Food and Drug Control, Nanning 530021, China.
FAU - Shi, Xiaoguang
AU  - Shi X
AD  - Guangxi Institute for Food and Drug Control, Nanning 530021, China.
FAU - Lu, Yixiang
AU  - Lu Y
AD  - Guangxi Institute for Food and Drug Control, Nanning 530021, China. 
      186424006@qq.com.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Acetonitriles)
RN  - 0 (Nitrosamines)
RN  - Z072SB282N (acetonitrile)
SB  - IM
MH  - Acetonitriles
MH  - *Gas Chromatography-Mass Spectrometry
MH  - Limit of Detection
MH  - *Meat
MH  - Nitrosamines/*analysis
MH  - Tandem Mass Spectrometry
OTO - NOTNLM
OT  - N-nitrosamines
OT  - QuEChERS
OT  - gas chromatography-triple quadrupole mass spectrometry (GC-MS/MS)
OT  - sour meats
EDAT- 2017/10/20 06:00
MHDA- 2018/11/10 06:00
CRDT- 2017/10/20 06:00
PHST- 2017/10/20 06:00 [entrez]
PHST- 2017/10/20 06:00 [pubmed]
PHST- 2018/11/10 06:00 [medline]
AID - 10.3724/SP.J.1123.2017.06006 [doi]
PST - ppublish
SO  - Se Pu. 2017 Oct 8;35(10):1086-1093. doi: 10.3724/SP.J.1123.2017.06006.