PMID- 29048826
OWN - NLM
STAT- MEDLINE
DCOM- 20181109
LR  - 20181109
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 35
IP  - 8
DP  - 2017 Aug 8
TI  - [Rapid screening of acidity regulators in dairy by ion chromatography-high 
      resolution mass spectrometry].
PG  - 886-890
LID - 10.3724/SP.J.1123.2017.04012 [doi]
AB  - A method for screening of acidity regulators in dairy based on ion 
      chromatography-high resolution mass spectrometry technology (IC-HRMS) was set up. 
      The dairy samples were extracted by KOH (pH 7-8) and Oasis MAX SPE column, and 
      separated by a Dionex IonPac AS11-HC column (250 mmx4 mm). All the acidity 
      regulators were detected by Orbitrap full scan mode. Taking six organic acids as 
      an example, the calibration curves showed good linearities in the range of 
      0.05-5.00 mg/L, and the correlation coefficients (r) were higher than 0.99. By 
      detecting the spiked samples, the recoveries were in the range of 74.3%-115.5% 
      with the relative standard deviations (RSDs) between 0.64% and 4.81%. Malic acid, 
      citric acid, lactic acid, succinic acid and adipic acid could be detected by 
      IC-HRMS in the commercial dairy samples. The results indicate that the method is 
      simple, rapid and suitable for the qualitative screening of acidity regulators in 
      dairy products.
FAU - Yun, Huan
AU  - Yun H
AD  - Beijing Entry-Exit Inspection and Quarantine Bureau, Beijing 100026, China.
FAU - Liu, Xin
AU  - Liu X
AD  - Beijing Entry-Exit Inspection and Quarantine Bureau, Beijing 100026, China. 
      liuxin@bjciq.gov.cn.
FAU - Cui, Jie
AU  - Cui J
AD  - Beijing Industrial Technician College, Beijing 100023, China.
FAU - Yang, Jing
AU  - Yang J
AD  - Beijing Entry-Exit Inspection and Quarantine Bureau, Beijing 100026, China.
FAU - Liu, Ying
AU  - Liu Y
AD  - Beijing Entry-Exit Inspection and Quarantine Bureau, Beijing 100026, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Acids)
RN  - 0 (Ions)
RN  - 0 (Organic Chemicals)
SB  - IM
MH  - Acids/*analysis
MH  - *Chromatography
MH  - *Dairy Products
MH  - Ions
MH  - *Mass Spectrometry
MH  - Organic Chemicals
MH  - Spectrum Analysis
OTO - NOTNLM
OT  - acidity regulators
OT  - dairy
OT  - ion chromatography-high resolution mass spectrometry (IC-HRMS)
OT  - rapid screening
EDAT- 2017/10/20 06:00
MHDA- 2018/11/10 06:00
CRDT- 2017/10/20 06:00
PHST- 2017/10/20 06:00 [entrez]
PHST- 2017/10/20 06:00 [pubmed]
PHST- 2018/11/10 06:00 [medline]
AID - 10.3724/SP.J.1123.2017.04012 [doi]
PST - ppublish
SO  - Se Pu. 2017 Aug 8;35(8):886-890. doi: 10.3724/SP.J.1123.2017.04012.