PMID- 29048827
OWN - NLM
STAT- MEDLINE
DCOM- 20181109
LR  - 20181109
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 35
IP  - 8
DP  - 2017 Aug 8
TI  - [Simultaneous determination of 11 mycotoxins in feeds by high performance liquid 
      chromatography-tandem mass spectrometry].
PG  - 891-896
LID - 10.3724/SP.J.1123.2017.03042 [doi]
AB  - A high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) 
      method was developed for the simultaneous determination of 11 mycotoxins in 
      feeds. The samples were extracted with acetonitrile, then cleaned up by 
      multifunctional purification column filler and PRIME HLB solid phase extraction 
      column. The 11 mycotoxins were separated on an Agilent Zorbax SB-C18 column (150 
      mmx2.1 mm, 3.5 mu m) with gradient elution program, and methanol-5 mmol/L ammonium 
      acetate solution containing 0.1%(v/v) formic acid were used as mobile phases. The 
      target compounds were detected under electrospray ionization (ESI) both in 
      positive and negative modes with multiple reaction monitoring mode, and 
      quantified by internal standard method. The results indicated that the 11 
      mycotoxins showed good linear relationships in their respective linear ranges, 
      and the correlation coefficients were greater than 0.99. The limits of 
      quantification (LOQs) were between 2.0 and 50.0 mu g/kg. The average recoveries 
      were between 79.3% and 101.6% at three spiked levels (1, 2 and 5 times LOQs) with 
      relative standard deviations (RSDs) of 5.9%-13.2% (n=5). The method is simple, 
      rapid, sensitive, and can be used for the analysis of the 11 mycotoxins in feeds.
FAU - Wei, Yunji
AU  - Wei Y
AD  - State Key Laboratory of Feed Safety Testing(Huai'an), Huai'an Entry-Exit 
      Inspection and Quarantine Bureau, Huai'an 223001, China. jswyj_84@163.com.
FAU - Feng, Min
AU  - Feng M
AD  - State Key Laboratory of Feed Safety Testing(Huai'an), Huai'an Entry-Exit 
      Inspection and Quarantine Bureau, Huai'an 223001, China.
FAU - Zhu, Zhenyi
AU  - Zhu Z
AD  - State Key Laboratory of Feed Safety Testing(Huai'an), Huai'an Entry-Exit 
      Inspection and Quarantine Bureau, Huai'an 223001, China.
FAU - He, Jian
AU  - He J
AD  - State Key Laboratory of Feed Safety Testing(Huai'an), Huai'an Entry-Exit 
      Inspection and Quarantine Bureau, Huai'an 223001, China.
FAU - Shen, Jinrong
AU  - Shen J
AD  - State Key Laboratory of Feed Safety Testing(Huai'an), Huai'an Entry-Exit 
      Inspection and Quarantine Bureau, Huai'an 223001, China.
FAU - He, Zhenghe
AU  - He Z
AD  - State Key Laboratory of Feed Safety Testing(Huai'an), Huai'an Entry-Exit 
      Inspection and Quarantine Bureau, Huai'an 223001, China.
FAU - Qin, Xian
AU  - Qin X
AD  - State Key Laboratory of Feed Safety Testing(Huai'an), Huai'an Entry-Exit 
      Inspection and Quarantine Bureau, Huai'an 223001, China.
FAU - Zhou, Liying
AU  - Zhou L
AD  - Kunshan Entry-Exit Inspection and Quarantine Bureau, Kunshan 215300, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Mycotoxins)
SB  - IM
MH  - *Chromatography, High Pressure Liquid
MH  - Mycotoxins/*analysis
MH  - Solid Phase Extraction
MH  - *Tandem Mass Spectrometry
OTO - NOTNLM
OT  - feeds
OT  - high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS)
OT  - multifunctional purification column filler
OT  - mycotoxins
OT  - solid phase extraction (SPE)
EDAT- 2017/10/20 06:00
MHDA- 2018/11/10 06:00
CRDT- 2017/10/20 06:00
PHST- 2017/10/20 06:00 [entrez]
PHST- 2017/10/20 06:00 [pubmed]
PHST- 2018/11/10 06:00 [medline]
AID - 10.3724/SP.J.1123.2017.03042 [doi]
PST - ppublish
SO  - Se Pu. 2017 Aug 8;35(8):891-896. doi: 10.3724/SP.J.1123.2017.03042.