PMID- 29048856
OWN - NLM
STAT- MEDLINE
DCOM- 20190205
LR  - 20190215
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 35
IP  - 9
DP  - 2017 Sep 8
TI  - [Rapid determination of four phenolic environmental estrogen residues in cooking 
      oil by ultra-performance liquid chromatography-high resolution mass spectrometry 
      coupled with solid-phase extraction].
PG  - 980-986
LID - 10.3724/SP.J.1123.2017.06003 [doi]
AB  - A fast, sensitive and accurate method for the determination of trace bisphenol S 
      (BPS), bisphenol F (BPF), bisphenol A (BPA) and 4-nonylphenol (4-NP) in cooking 
      oil samples was developed by ultra-performance liquid chromatography-high 
      resolution mass spectrometry (UPLC-HRMS) coupled with solid-phase extraction 
      (SPE). Cooking oil samples were extracted by acetonitrile, then the supernatant 
      was purified by SLC SPE cartridges. The chromatographic separation was carried 
      out on a Waters ACQUITY UPLC HSS T(3) column (100 mmx2.1 mm, 1.8 mum) with a 
      linear gradient elution procedure using 0.05% (v/v) triethanolamine aqueous 
      solution and methanol as mobile phases. The quantification analysis was operated 
      in a negative electrospray ion (ESI(-)) source mode under the selected ion 
      monitoring (SIM) mode with internal standard method. The four target analytes 
      showed good linearity with correlation coefficients (r) greater than 0.999. The 
      limits of detection (LODs, S/N=3) and limits of quantification (LOQs, S/N=10) 
      were in the ranges of 0.03-0.11 mug/kg and 0.10-0.36 mug/kg, respectively. The 
      recoveries of the four target analytes spiked in oil samples were in the range of 
      86.3%-96.1% at spiked levels of 1.0, 10.0 and 80.0 mug/kg, respectively, while the 
      relative standard deviations (RSDs) were in range of 2.2%-8.8% (n=6). No 
      significant matrix interference was found in this method. The proposed method is 
      simple and fast. It can be applied for the rapid determination of trace BPS, BPF, 
      BPA, and 4-NP in cooking oil samples.
FAU - Pan, Shengdong
AU  - Pan S
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Key Laboratory of Poison Research and Control, Ningbo Municipal 
      Center for Disease Control and Prevention, Ningbo 315010, China.
FAU - He, Qian
AU  - He Q
AD  - National Institute of Occupational Health and Poison Control, Chinese Center for 
      Disease Control and Prevention, Beijing 100050, China.
FAU - Chen, Xiaohong
AU  - Chen X
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Key Laboratory of Poison Research and Control, Ningbo Municipal 
      Center for Disease Control and Prevention, Ningbo 315010, China.
FAU - Wang, Li
AU  - Wang L
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Key Laboratory of Poison Research and Control, Ningbo Municipal 
      Center for Disease Control and Prevention, Ningbo 315010, China.
FAU - Qiu, Qiaoli
AU  - Qiu Q
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Key Laboratory of Poison Research and Control, Ningbo Municipal 
      Center for Disease Control and Prevention, Ningbo 315010, China.
FAU - Jin, Micong
AU  - Jin M
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Key Laboratory of Poison Research and Control, Ningbo Municipal 
      Center for Disease Control and Prevention, Ningbo 315010, China. jmcjc@163.com.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Benzhydryl Compounds)
RN  - 0 (Dietary Fats, Unsaturated)
RN  - 0 (Estrogens)
RN  - 0 (Phenols)
RN  - 0 (Sulfones)
RN  - 0 (bisphenol F)
RN  - 80-09-1 (bis(4-hydroxyphenyl)sulfone)
RN  - I03GBV4WEL (4-nonylphenol)
RN  - MLT3645I99 (bisphenol A)
SB  - IM
MH  - Benzhydryl Compounds/analysis
MH  - *Chromatography, High Pressure Liquid
MH  - Cooking
MH  - Dietary Fats, Unsaturated/*analysis
MH  - Estrogens/*analysis
MH  - Food Contamination/*analysis
MH  - Phenols/analysis
MH  - Solid Phase Extraction
MH  - Sulfones/analysis
MH  - *Tandem Mass Spectrometry
OTO - NOTNLM
OT  - 4-nonylphenol (4-NP)
OT  - bisphenol A (BPA)
OT  - bisphenol F (BPF)
OT  - bisphenol S (BPS)
OT  - cooking oil
OT  - phenolic environmental estrogens
OT  - solid-phase extraction (SPE)
OT  - ultra-performance liquid chromatography-high resolution mass spectrometry 
      (UPLC-HRMS)
EDAT- 2017/10/20 06:00
MHDA- 2019/02/06 06:00
CRDT- 2017/10/20 06:00
PHST- 2017/10/20 06:00 [entrez]
PHST- 2017/10/20 06:00 [pubmed]
PHST- 2019/02/06 06:00 [medline]
AID - 10.3724/SP.J.1123.2017.06003 [doi]
PST - ppublish
SO  - Se Pu. 2017 Sep 8;35(9):980-986. doi: 10.3724/SP.J.1123.2017.06003.