PMID- 29120796 OWN - NLM STAT- MEDLINE DCOM- 20180813 LR - 20181202 IS - 1873-7072 (Electronic) IS - 0308-8146 (Linking) VI - 244 DP - 2018 Apr 1 TI - A rapid and simple HPLC-FLD screening method with QuEChERS as the sample treatment for the simultaneous monitoring of nine bisphenols in milk. PG - 371-377 LID - S0308-8146(17)31659-X [pii] LID - 10.1016/j.foodchem.2017.10.030 [doi] AB - A specific, precise and accurate high performance liquid chromatographic (HPLC) analytical method with a fluorescence detector (FLD) was established for the simultaneous determination of nine bisphenols (BPs) in milk samples. Samples were extracted ultrasonically with acetonitrile and cleaned using the QuEChERS technique. Under the optimized conditions, good linearity was obtained for the nine BPs and the correlation coefficients (R(2)) ranged from 0.9942 to 0.9997. Recovery values for the nine bisphenols in spiked samples were 75.82-93.86% with intra-day and inter-day relative standard deviations (RSDs) from 2.6 to 11.1%. The limits of detection (LODs) and quantification (LOQs) were 1.0-3.1 mug/kg and 3.5-9.8 mug/kg, respectively. The results demonstrated clearly that the approach developed provides reliable, simple, rapid and environmentally-friendly quantification and identification of nine bisphenols in a fatty matrix and could be used for monitoring bisphenols in milk. CI - Copyright (c) 2017 Elsevier Ltd. All rights reserved. FAU - Xiong, Lin AU - Xiong L AD - Lanzhou Institute of Husbandry and Pharmaceutical Sciences, Chinese Academy of Agricultural Sciences, Lanzhou 730050 Gansu, China; Laboratory of Quality & Safety Risk Assessment for Livestock Product (Lanzhou), Ministry of Agriculture, Lanzhou 730050 Gansu, China. Electronic address: xionglin807@sina.com. FAU - Yan, Ping AU - Yan P AD - Lanzhou Institute of Husbandry and Pharmaceutical Sciences, Chinese Academy of Agricultural Sciences, Lanzhou 730050 Gansu, China; Laboratory of Quality & Safety Risk Assessment for Livestock Product (Lanzhou), Ministry of Agriculture, Lanzhou 730050 Gansu, China; Key Laboratory for Yak Genetics, Breeding & Reproduction Engineering of Gansu Province, Lanzhou 730050 Gansu, China. FAU - Chu, Min AU - Chu M AD - Lanzhou Institute of Husbandry and Pharmaceutical Sciences, Chinese Academy of Agricultural Sciences, Lanzhou 730050 Gansu, China; Key Laboratory for Yak Genetics, Breeding & Reproduction Engineering of Gansu Province, Lanzhou 730050 Gansu, China. FAU - Gao, Ya-Qin AU - Gao YQ AD - Lanzhou Institute of Husbandry and Pharmaceutical Sciences, Chinese Academy of Agricultural Sciences, Lanzhou 730050 Gansu, China; Laboratory of Quality & Safety Risk Assessment for Livestock Product (Lanzhou), Ministry of Agriculture, Lanzhou 730050 Gansu, China. FAU - Li, Wei-Hong AU - Li WH AD - Lanzhou Institute of Husbandry and Pharmaceutical Sciences, Chinese Academy of Agricultural Sciences, Lanzhou 730050 Gansu, China; Laboratory of Quality & Safety Risk Assessment for Livestock Product (Lanzhou), Ministry of Agriculture, Lanzhou 730050 Gansu, China. FAU - Yang, Xiao-Ling AU - Yang XL AD - Lanzhou Institute of Husbandry and Pharmaceutical Sciences, Chinese Academy of Agricultural Sciences, Lanzhou 730050 Gansu, China; Laboratory of Quality & Safety Risk Assessment for Livestock Product (Lanzhou), Ministry of Agriculture, Lanzhou 730050 Gansu, China. LA - eng PT - Journal Article DEP - 20171010 PL - England TA - Food Chem JT - Food chemistry JID - 7702639 RN - 0 (Benzhydryl Compounds) RN - 0 (Phenols) RN - 1RC731TJJA (bisphenol B) RN - MLT3645I99 (bisphenol A) SB - IM MH - Animals MH - Benzhydryl Compounds/analysis MH - Chromatography, High Pressure Liquid/*methods MH - Fluorescence MH - Food Analysis/*methods MH - Food Contamination/*analysis MH - Limit of Detection MH - Milk/*chemistry MH - Phenols/*analysis OTO - NOTNLM OT - Bisphenol A (PubChem CID: 6623) OT - Bisphenol A Bis (2, 3-dihydroxyprophy) Ether (PubChem CID: 110678) OT - Bisphenol A diglycidyl ether (PubChem CID: 2286) OT - Bisphenol B (PubChem CID: 66166) OT - Bisphenol C (PubChem CID: 6620) OT - Bisphenol E (PubChem CID: 608116) OT - Bisphenol F Diglycidyl Ether (PubChem CID: 91511) OT - Bisphenol F Glycidyl 2,3-Dihydroxypropyl Ether (PubChem CID: 71360307) OT - Bisphenol F bis (2,3-dihydroxyprophy) Ether (PubChem CID: 3928015) OT - Bisphenols OT - HPLC-FLD OT - Milk OT - QuEChERS EDAT- 2017/11/10 06:00 MHDA- 2018/08/14 06:00 CRDT- 2017/11/10 06:00 PHST- 2016/10/19 00:00 [received] PHST- 2017/08/23 00:00 [revised] PHST- 2017/10/08 00:00 [accepted] PHST- 2017/11/10 06:00 [entrez] PHST- 2017/11/10 06:00 [pubmed] PHST- 2018/08/14 06:00 [medline] AID - S0308-8146(17)31659-X [pii] AID - 10.1016/j.foodchem.2017.10.030 [doi] PST - ppublish SO - Food Chem. 2018 Apr 1;244:371-377. doi: 10.1016/j.foodchem.2017.10.030. Epub 2017 Oct 10.