PMID- 29713431 OWN - NLM STAT- PubMed-not-MEDLINE LR - 20231112 IS - 2005-7806 (Print) IS - 2005-7814 (Electronic) IS - 2005-7806 (Linking) VI - 10 IP - 2 DP - 2018 Apr TI - Effects of incorporation of 2.5 and 5 wt% TiO(2) nanotubes on fracture toughness, flexural strength, and microhardness of denture base poly methyl methacrylate (PMMA). PG - 113-121 LID - 10.4047/jap.2018.10.2.113 [doi] AB - PURPOSE: The aim of this preliminary study was to investigate, for the first time, the effects of addition of titania nanotubes (n-TiO(2)) to poly methyl methacrylate (PMMA) on mechanical properties of PMMA denture base. MATERIALS AND METHODS: TiO(2) nanotubes were prepared using alkaline hydrothermal process. Obtained nanotubes were assessed using FESEM-EDX, XRD, and FT-IR. For 3 experiments of this study (fracture toughness, three-point bending flexural strength, and Vickers microhardness), 135 specimens were prepared according to ISO 20795-1:2013 (n of each experiment=45). For each experiment, PMMA was mixed with 0% (control), 2.5 wt%, and 5 wt% nanotubes. From each TiO(2):PMMA ratio, 15 specimens were fabricated for each experiment. Effects of n-TiO(2) addition on 3 mechanical properties were assessed using Pearson, ANOVA, and Tukey tests. RESULTS: SEM images of n-TiO(2) exhibited the presence of elongated tubular structures. The XRD pattern of synthesized n-TiO(2) represented the anatase crystal phase of TiO(2). Moderate to very strong significant positive correlations were observed between the concentration of n-TiO(2) and each of the 3 physicomechanical properties of PMMA (Pearson's P value