PMID- 30015566
OWN - NLM
STAT- MEDLINE
DCOM- 20190408
LR  - 20190408
IS  - 1532-4109 (Electronic)
IS  - 0360-1234 (Linking)
VI  - 53
IP  - 11
DP  - 2018
TI  - Magnetic molecularly imprinted polymer prepared by microwave heating for 
      confirmatory determination of chloramphenicol in chicken feed using 
      high-performance liquid chromatography-tandem mass spectrometry.
PG  - 738-745
LID - 10.1080/03601234.2018.1480161 [doi]
AB  - A magnetic molecularly imprinted polymer (MMIP) for chloramphenicol was prepared 
      using a surface-imprinted and microwave-heating-induced polymerization method. 
      The surfaces of the magnetic particles were first double-bond functionalized with 
      3-(trimethoxysilyl)propyl methacrylate (gamma-MPS), followed by the copolymerization 
      of 4-vinyl pyridine (4-VP) and trimethylolpropane trimethacrylate (TRIM) in the 
      presence of chloramphenicol as a template and 
      1,1-azobis(cyclohexane-carbonitrile) (ABCN) as an initiator in a mixture of 
      dimethyl sulfoxide and water with microwave heating at 80 degrees C. The magnetic polymer 
      possesses supraparamagnetic properties and was used to concentrate and cleanup 
      chicken feed extract, followed by chromatographic separation using a 
      Lichrospher(R)100 RP C8 column and detection with two multi-reaction monitoring 
      transitions at m/z 321--> 152 and m/z 321--> 257. The mean recoveries obtained at two 
      spiking levels were in the range of 94.6-100% The relative intra- and inter-day 
      standard deviations were in the range of 1.4-2.6% and 5.1-5.7%, respectively. The 
      detection limit of the method was 0.12 microg kg(-1). This confirmatory method was 
      successfully applied to determine chloramphenicol in chicken feed samples.
FAU - Kunsa-Ngiem, Sumate
AU  - Kunsa-Ngiem S
AD  - a Department of Chemistry and Center for Innovation in Chemistry , Faculty of 
      Science, Kasetsart University , Bangkok , Thailand.
FAU - Sutthivaiyakit, Pakawadee
AU  - Sutthivaiyakit P
AD  - a Department of Chemistry and Center for Innovation in Chemistry , Faculty of 
      Science, Kasetsart University , Bangkok , Thailand.
FAU - Lowmunkhong, Pongsak
AU  - Lowmunkhong P
AD  - a Department of Chemistry and Center for Innovation in Chemistry , Faculty of 
      Science, Kasetsart University , Bangkok , Thailand.
FAU - Harir, Mourad
AU  - Harir M
AD  - b Helmholtz Zentrum Munchen, German Research Center for Environmental Health , 
      Research Unit Analytical BioGeoChemistry , Neuherberg , Germany.
AD  - c Chair of Analytical Food Chemistry , Technische Universitat Munchen , 
      Freising-Weihenstephan , Germany.
FAU - Schmitt-Kopplin, Philippe
AU  - Schmitt-Kopplin P
AD  - b Helmholtz Zentrum Munchen, German Research Center for Environmental Health , 
      Research Unit Analytical BioGeoChemistry , Neuherberg , Germany.
AD  - c Chair of Analytical Food Chemistry , Technische Universitat Munchen , 
      Freising-Weihenstephan , Germany.
FAU - Sutthivaiyakit, Somyote
AU  - Sutthivaiyakit S
AD  - d Department of Chemistry and Center of Excellence for Innovation in Chemistry , 
      Faculty of Science, Ramkhamhaeng University , Bangkok , Thailand .
LA  - eng
PT  - Journal Article
DEP - 20180717
PL  - England
TA  - J Environ Sci Health B
JT  - Journal of environmental science and health. Part. B, Pesticides, food 
      contaminants, and agricultural wastes
JID - 7607167
RN  - 0 (Methacrylates)
RN  - 0 (Polymers)
RN  - 0 (Pyridines)
RN  - 66974FR9Q1 (Chloramphenicol)
RN  - I56G67XM8D (4-vinylpyridine)
RN  - S734UC120F (trimethylolpropane trimethacrylate)
SB  - IM
EIN - J Environ Sci Health B. 2019;54(1):76. PMID: 30757961
MH  - Animal Feed/*analysis
MH  - Animals
MH  - Chickens
MH  - Chloramphenicol/*analysis/chemistry
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Heating
MH  - Limit of Detection
MH  - Methacrylates/chemistry
MH  - Microwaves
MH  - Molecular Imprinting
MH  - Polymers/*chemistry
MH  - Pyridines/chemistry
MH  - Solid Phase Extraction/methods
MH  - Tandem Mass Spectrometry/*methods
OTO - NOTNLM
OT  - Chicken feed
OT  - chloramphenicol
OT  - magnetic molecularly imprinted polymers
OT  - microwave heating
EDAT- 2018/07/18 06:00
MHDA- 2019/04/09 06:00
CRDT- 2018/07/18 06:00
PHST- 2018/07/18 06:00 [pubmed]
PHST- 2019/04/09 06:00 [medline]
PHST- 2018/07/18 06:00 [entrez]
AID - 10.1080/03601234.2018.1480161 [doi]
PST - ppublish
SO  - J Environ Sci Health B. 2018;53(11):738-745. doi: 10.1080/03601234.2018.1480161. 
      Epub 2018 Jul 17.