PMID- 30086894
OWN - NLM
STAT- MEDLINE
DCOM- 20181026
LR  - 20181026
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 189
DP  - 2018 Nov 1
TI  - A novel air-assisted liquid-liquid microextraction based on in-situ phase 
      separation for the HPLC determination of bisphenols migration from disposable 
      lunch boxes to contacting water.
PG  - 116-121
LID - S0039-9140(18)30677-5 [pii]
LID - 10.1016/j.talanta.2018.06.072 [doi]
AB  - In this study, a novel air-assisted liquid-liquid microextraction (AALLME) method 
      was developed for the HPLC determination of bisphenols migration from disposable 
      plastic lunch box to contacting water. The AALLME was carried out in 
      commercially-available medical plastic syringes with low-density extraction 
      solvent (n-octanol), and the reaction of NaHCO(3) and HCl was introduced to 
      simultaneously induce the in-situ phase separation and salt effect. After the 
      AALLME processes, the upper organic phase was pushed into the end of syringes 
      (narrow tube) by moving the piston so that it could be readily collected for the 
      HPLC analysis. The factors including the type and volume of extraction solvent, 
      NaHCO(3) addition and extraction cycles were optimized. Under the optimal 
      conditions, the limits of detection (LODs) for target bisphenols were evaluated 
      to be 0.2-0.7 mug L(-1), and good linearities with correlation coefficients higher 
      than 0.9955 were obtained. The recoveries for target bisphenols ranged from 80% 
      to 106%, with the relative standard deviations (RSDs) of 4.4-14.1%. The proposed 
      method was successfully applied to investigate the migration of bisphenols from 
      the disposable plastic lunch boxes to the contacting water, revealing that 
      compared to the conventional water-bath heating, the microwave heating could 
      induce the significant migration of bisphenols in a much shorter time.
CI  - Copyright (c) 2018 Elsevier B.V. All rights reserved.
FAU - Zhou, Qinghua
AU  - Zhou Q
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, China.
FAU - Jin, Zanhui
AU  - Jin Z
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, China.
FAU - Li, Jia
AU  - Li J
AD  - Key Laboratory of Tea Biology and Resources Utilization, Ministry of Agriculture, 
      Tea Research Institute, Chinese Academy of Agricultural Sciences, Hangzhou 
      310008, China.
FAU - Wang, Bin
AU  - Wang B
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, China.
FAU - Wei, Xiuzhen
AU  - Wei X
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, China.
FAU - Chen, Jinyuan
AU  - Chen J
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, China. Electronic address: jyc1128@126.com.
LA  - eng
PT  - Journal Article
DEP - 20180625
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
RN  - 0 (Phenols)
RN  - 0 (Plastics)
RN  - 0 (Solvents)
RN  - 059QF0KO0R (Water)
RN  - 8MDF5V39QO (Sodium Bicarbonate)
SB  - IM
MH  - *Air
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Food Contamination/analysis
MH  - Limit of Detection
MH  - Liquid Phase Microextraction/*methods
MH  - *Lunch
MH  - Phenols/*analysis/chemistry/*isolation & purification
MH  - Plastics/chemistry
MH  - Sodium Bicarbonate/chemistry
MH  - Solvents/chemistry
MH  - Water/*chemistry
OTO - NOTNLM
OT  - Air-assisted liquid-liquid microextraction
OT  - Bisphenols
OT  - Disposable lunch boxes
OT  - High performance liquid chromatography
OT  - Migration
EDAT- 2018/08/09 06:00
MHDA- 2018/10/27 06:00
CRDT- 2018/08/09 06:00
PHST- 2018/04/10 00:00 [received]
PHST- 2018/05/31 00:00 [revised]
PHST- 2018/06/24 00:00 [accepted]
PHST- 2018/08/09 06:00 [entrez]
PHST- 2018/08/09 06:00 [pubmed]
PHST- 2018/10/27 06:00 [medline]
AID - S0039-9140(18)30677-5 [pii]
AID - 10.1016/j.talanta.2018.06.072 [doi]
PST - ppublish
SO  - Talanta. 2018 Nov 1;189:116-121. doi: 10.1016/j.talanta.2018.06.072. Epub 2018 
      Jun 25.