PMID- 30136475
OWN - NLM
STAT- MEDLINE
DCOM- 20181017
LR  - 20210702
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 36
IP  - 6
DP  - 2018 Jun 8
TI  - [Determination of cinnamaldehyde residues in fresh fruits and meats by modified 
      QuEChERS combined with gas chromatography-tandem mass spectrometry].
PG  - 541-546
LID - 10.3724/SP.J.1123.2017.11035 [doi]
AB  - A method for the determination of cinnamaldehyde residues in fresh fruits and 
      meats by gas chromatography-tandem mass spectrometry (GC-MS) coupled with 
      modified QuEChERS was developed. The samples were extracted with ethyl acetate. 
      Solid phase extraction agents such as graphitized carbon black (GCB), 
      primary-secondary amine (PSA) and octadecyl bonded silica (C(18)) were used for 
      adsorption and purification. The extracts were detected by electron impact 
      ionization in selected ion monitoring (SIM) mode and quantified using external 
      standard method. The results revealed correlation coefficients (R(2)) greater 
      than 0.999 in the range of 0.01-0.5 mg/L. The limits of quantification (LOQs) 
      were 0.05 to 0.1 mg/kg. The recoveries at the three spiked levels ranged from 
      81.9% to 104.5% with the relative standard deviations (RSDs) ranging from 1.1% to 
      8.6%. The proposed method is efficient, sensitive, reliable, and is suitable for 
      the trace determination of the cinnamaldehyde residues in fresh fruits and meats.
FAU - Liu, Ying
AU  - Liu Y
AD  - Inspection and Quarantine Technical Center of Beijing Entry-Exit Inspection and 
      Quarantine Bureau, Beijing 100026, China.
FAU - Zhang, Rong
AU  - Zhang R
AD  - Inspection and Quarantine Technical Center of Beijing Entry-Exit Inspection and 
      Quarantine Bureau, Beijing 100026, China.
FAU - Cui, Fengyun
AU  - Cui F
AD  - Inspection and Quarantine Technical Center of Beijing Entry-Exit Inspection and 
      Quarantine Bureau, Beijing 100026, China.
FAU - Han, Shen
AU  - Han S
AD  - Inspection and Quarantine Technical Center of Beijing Entry-Exit Inspection and 
      Quarantine Bureau, Beijing 100026, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 7864XYD3JJ (Acrolein)
RN  - SR60A3XG0F (cinnamaldehyde)
SB  - IM
MH  - Acrolein/*analogs & derivatives/analysis
MH  - Fruit/*chemistry
MH  - Gas Chromatography-Mass Spectrometry
MH  - Meat/*analysis
MH  - Solid Phase Extraction
MH  - Tandem Mass Spectrometry
OTO - NOTNLM
OT  - QuEChERS
OT  - cinnamaldehyde
OT  - fruit
OT  - gas chromatography-tandem mass spectrometry (GC-MS)
OT  - meat
EDAT- 2018/08/24 06:00
MHDA- 2018/10/18 06:00
CRDT- 2018/08/24 06:00
PHST- 2018/08/24 06:00 [entrez]
PHST- 2018/08/24 06:00 [pubmed]
PHST- 2018/10/18 06:00 [medline]
AID - 10.3724/SP.J.1123.2017.11035 [doi]
PST - ppublish
SO  - Se Pu. 2018 Jun 8;36(6):541-546. doi: 10.3724/SP.J.1123.2017.11035.