PMID- 30158395
OWN - NLM
STAT- MEDLINE
DCOM- 20190621
LR  - 20190621
IS  - 0015-6426 (Print)
IS  - 0015-6426 (Linking)
VI  - 59
IP  - 4
DP  - 2018
TI  - [Determination of Hexazinone and Its Major Metabolites in Livestock Products by 
      LC-MS/MS].
PG  - 167-173
LID - 10.3358/shokueishi.59.167 [doi]
AB  - A method for the determination of hexazinone and three metabolites (hexazinone 
      metabolite B, hexazinone metabolite C, hexazinone metabolite F) in livestock 
      products by LC-MS/MS was developed. Hexazinone and the three metabolites were 
      extracted from a sample with acetonitrile in the presence of n-hexane, and lipid 
      was removed by acetonitrile/n-hexane partition. The acetonitrile extract was 
      cleaned up using a SAX/PSA cartridge column. Average recoveries (n=5) of 
      hexazinone and the three metabolites from cattle meat, fat, liver and milk spiked 
      at the maximum residue limits (MRLs) or at 0.0025 mg/kg ranged from 85.6 to 
      96.0%, and the relative standard deviations ranged from 0.8 to 4.9%.
FAU - Kubota, Akiko
AU  - Kubota A
AD  - Hokkaido Institute of Public Health.
FAU - Okabe, Ryo
AU  - Okabe R
AD  - Hokkaido Institute of Public Health.
FAU - Kakimoto, Youichiro
AU  - Kakimoto Y
AD  - Hokkaido Institute of Public Health.
FAU - Nemoto, Satoru
AU  - Nemoto S
AD  - National Institute of Health Sciences.
FAU - Aoyagi, Mitsutoshi
AU  - Aoyagi M
AD  - Hokkaido Institute of Public Health.
LA  - jpn
PT  - Journal Article
PL  - Japan
TA  - Shokuhin Eiseigaku Zasshi
JT  - Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan
JID - 0142214
RN  - 0 (Triazines)
RN  - Y51727MR1Y (hexazinone)
SB  - IM
MH  - Animals
MH  - Cattle
MH  - Chromatography, Liquid
MH  - Dairy Products/*analysis
MH  - Meat Products/*analysis
MH  - Milk/*chemistry
MH  - Tandem Mass Spectrometry
MH  - Triazines/*analysis
OTO - NOTNLM
OT  - LC-MS/MS
OT  - herbicide
OT  - hexazinone
OT  - livestock products
OT  - major metabolites
EDAT- 2018/08/31 06:00
MHDA- 2019/06/22 06:00
CRDT- 2018/08/31 06:00
PHST- 2018/08/31 06:00 [entrez]
PHST- 2018/08/31 06:00 [pubmed]
PHST- 2019/06/22 06:00 [medline]
AID - 10.3358/shokueishi.59.167 [doi]
PST - ppublish
SO  - Shokuhin Eiseigaku Zasshi. 2018;59(4):167-173. doi: 10.3358/shokueishi.59.167.