PMID- 30248772 OWN - NLM STAT- MEDLINE DCOM- 20181015 LR - 20181023 IS - 1001-9391 (Print) IS - 1001-9391 (Linking) VI - 36 IP - 7 DP - 2018 Jul 20 TI - [Direct determination of manganese in urine by Graphite Furnace Atomic Absorption Spectrometry]. PG - 535-537 LID - 10.3760/cma.j.issn.1001-9391.2018.07.016 [doi] AB - Objective: To establish a method for the determination of manganese in urine by graphite furnace atomic absorption spectrometry (AAS) without the use of matrix modifier. Methods: The urine samples were 5 times diluted with 1% nitric acid then directly determined by AAS. Zeeman was used for background correction. Results: The linear range for determination of manganese in urine was 5~60 mug/L (urine) . The correlation coefficient was greater than 0.995 with the detection limit of 1.5 mug/L and with the lower limit of quantification of 5.0 mug/L. The relative standard deviations (RSDs) of within-run precision was between 1.1%~4.3%, the RSDs of between-run precision was between 3.3%~7.0%. The average recovery was 102.6%. The samples can be stored for 14 days at room temperature, 4℃, -8 ℃ and -35 ℃. Conclusion: The method is feasible for determination of manganese in urine. FAU - Lin, Y R AU - Lin YR AD - Shenzhen Prevention and Treatment center for Occupational Diseases, Shenzhen 518001, China. FAU - Li, T D AU - Li TD FAU - Zhang, W AU - Zhang W FAU - Yun, J P AU - Yun JP FAU - Liu, F AU - Liu F FAU - Huang, X Q AU - Huang XQ LA - chi PT - Journal Article PL - China TA - Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi JT - Zhonghua lao dong wei sheng zhi ye bing za zhi = Zhonghua laodong weisheng zhiyebing zazhi = Chinese journal of industrial hygiene and occupational diseases JID - 8410840 RN - 0 (Biomarkers) RN - 411VRN1TV4 (Nitric Acid) RN - 42Z2K6ZL8P (Manganese) RN - 7782-42-5 (Graphite) SB - IM MH - Biomarkers/urine MH - Graphite/*chemistry MH - Humans MH - Limit of Detection MH - Manganese/*urine MH - Nitric Acid MH - Spectrophotometry, Atomic/*methods OTO - NOTNLM OT - AAS OT - manganese in urine EDAT- 2018/09/27 06:00 MHDA- 2018/10/16 06:00 CRDT- 2018/09/25 06:00 PHST- 2018/09/25 06:00 [entrez] PHST- 2018/09/27 06:00 [pubmed] PHST- 2018/10/16 06:00 [medline] AID - 10.3760/cma.j.issn.1001-9391.2018.07.016 [doi] PST - ppublish SO - Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi. 2018 Jul 20;36(7):535-537. doi: 10.3760/cma.j.issn.1001-9391.2018.07.016.