PMID- 30251507
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20180926
LR  - 20180926
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 36
IP  - 8
DP  - 2018 Aug 8
TI  - [Determination of aminobutanol by high performance liquid chromatography based on 
      charge transfer reaction].
PG  - 817-821
LID - 10.3724/SP.J.1123.2018.03026 [doi]
AB  - A method was developed for the determination of the content of aminobutanol by 
      high performance liquid chromatography (HPLC) based on charge transfer reaction. 
      Under the condition of a borax-boric acid buffer solution of pH 8.4, aminobutanol 
      and tetra-chloro-benzoquinone reacted at 60℃ for 60 min, and were analyzed by an 
      HPLC-ultraviolet detector. The charge-transfer complex was separated on an 
      Agilent Extend C18 column (250 mmx4.6 mm, 5 mum) with 0.001% (v/v) triethylamine 
      and methanol as the mobile phases for gradient elution at a flow rate of 1 
      mL/min. The limit of quantification of aminobutanol was 0.01 g/L, the linear 
      range was 0.1-0.6 g/L, and the correlation coefficient (R(2)) was 0.9994. The 
      spiked recoveries of the method were 98.3%-103.6% with relative standard 
      deviations (RSDs) of 0.9%-1.6%. The method is simple and quick, and suitable for 
      the rapid detection of aminobutanol.
FAU - Shao, Meiqi
AU  - Shao M
AD  - Zhejiang University of Technology, Collaborative Innovation Center of Yangtze 
      River Delta Region Green Pharmaceuticals, Hangzhou 310014, China.
FAU - Chen, Yan
AU  - Chen Y
AD  - Zhejiang University of Technology, Collaborative Innovation Center of Yangtze 
      River Delta Region Green Pharmaceuticals, Hangzhou 310014, China.
FAU - Peng, Qing
AU  - Peng Q
AD  - Zhejiang University of Technology, Collaborative Innovation Center of Yangtze 
      River Delta Region Green Pharmaceuticals, Hangzhou 310014, China.
FAU - Liu, Pengfu
AU  - Liu P
AD  - Zhejiang University of Technology, Collaborative Innovation Center of Yangtze 
      River Delta Region Green Pharmaceuticals, Hangzhou 310014, China.
AD  - Zhejiang Yangtze Delta Region Pharmaceutical Technology Research Park, Deqing 
      313200, China.
FAU - Wu, Jiequn
AU  - Wu J
AD  - Zhejiang University of Technology, Collaborative Innovation Center of Yangtze 
      River Delta Region Green Pharmaceuticals, Hangzhou 310014, China.
AD  - Zhejiang Yangtze Delta Region Pharmaceutical Technology Research Park, Deqing 
      313200, China.
FAU - Chu, Xiaohe
AU  - Chu X
AD  - Zhejiang University of Technology, Collaborative Innovation Center of Yangtze 
      River Delta Region Green Pharmaceuticals, Hangzhou 310014, China.
AD  - Zhejiang Yangtze Delta Region Pharmaceutical Technology Research Park, Deqing 
      313200, China.
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
OTO - NOTNLM
OT  - aminobutanol
OT  - charge transfer reaction
OT  - high performance liquid chromatography (HPLC)
OT  - tetra-chloro-benzoquinone (TCBQ)
EDAT- 2018/09/27 06:00
MHDA- 2018/09/27 06:01
CRDT- 2018/09/26 06:00
PHST- 2018/09/26 06:00 [entrez]
PHST- 2018/09/27 06:00 [pubmed]
PHST- 2018/09/27 06:01 [medline]
AID - 10.3724/SP.J.1123.2018.03026 [doi]
PST - ppublish
SO  - Se Pu. 2018 Aug 8;36(8):817-821. doi: 10.3724/SP.J.1123.2018.03026.