PMID- 30360133
OWN - NLM
STAT- MEDLINE
DCOM- 20210531
LR  - 20210531
IS  - 1533-4880 (Print)
IS  - 1533-4880 (Linking)
VI  - 19
IP  - 2
DP  - 2019 Feb 1
TI  - Synthesis of MOF-199/CNTs Nanocomposite for Selective Adsorption and 
      Determination of Nonsteroidal Anti-Inflammatory Drugs in Human Urine.
PG  - 627-633
LID - 10.1166/jnn.2019.15733 [doi]
AB  - A hybrid nanocomposite containing a moisture-resistant surface based on MOF-199 
      and carbon nanotubes (CNTs) was synthesized. Characterization was undertaken 
      using powder X-ray diffraction (PXRD), scanning electron microscopy (SEM) and 
      Fourier transform infrared spectroscopy (FT-IR). The adsorption behavior of the 
      MOF-199/CNTs composite to ibuprofen was then investigated at room temperature. 
      Experimentation revealed that the hybrid absorbent had excellent adsorption 
      capacity for the nonsteroidal anti-inflammatory drug (NSAID), ibuprofen, with 
      maximum adsorption up to 40.8 mg/g. The adsorbent was able to be recycled several 
      times without deactivation. Finally, the MOF-199/CNTs composite was used as the 
      extraction sorbents for selective extraction of ibuprofen, ketoprofen and 
      naproxen in human urine. The results showed successful application of the 
      nanocomposite to NSAID analysis in spiked human urine samples. Recoveries at 
      three concentrations were 89.7-96.8%, 79.3-85.5% and 95.6-97.5% for ibuprofen, 
      ketoprofen and naproxen, respectively. The relative standard deviations (RSDs) 
      were within the range of 2.9-5.3%. The results demonstrated that the MOF-199/CNTs 
      composite is an excellent adsorbent for determination of NSAIDs in spiked urine 
      samples.
FAU - Wang, Xiaobing
AU  - Wang X
AD  - College of Chemistry and Environmental Engineering, Shaoguan University, Shaoguan 
      512005, China.
FAU - Zhu, Huijuan
AU  - Zhu H
AD  - College of Chemistry and Environmental Engineering, Shaoguan University, Shaoguan 
      512005, China.
FAU - Shi, Xiuyi
AU  - Shi X
AD  - College of Chemistry and Environmental Engineering, Shaoguan University, Shaoguan 
      512005, China.
FAU - Qiu, Xiuzhen
AU  - Qiu X
AD  - College of Chemistry and Environmental Engineering, Shaoguan University, Shaoguan 
      512005, China.
FAU - Lu, Wenguan
AU  - Lu W
AD  - College of Chemistry and Environmental Engineering, Shaoguan University, Shaoguan 
      512005, China.
FAU - Guo, Huishi
AU  - Guo H
AD  - College of Chemistry and Environmental Engineering, Shaoguan University, Shaoguan 
      512005, China.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - United States
TA  - J Nanosci Nanotechnol
JT  - Journal of nanoscience and nanotechnology
JID - 101088195
RN  - 0 (Anti-Inflammatory Agents, Non-Steroidal)
RN  - 0 (Metal-Organic Frameworks)
RN  - 0 (Nanotubes, Carbon)
RN  - 0 (Pharmaceutical Preparations)
RN  - 0 (bis(1,3,5-benzenetricarboxylate)tricopper(II))
SB  - IM
MH  - Adsorption
MH  - Anti-Inflammatory Agents, Non-Steroidal
MH  - Humans
MH  - Metal-Organic Frameworks
MH  - *Nanocomposites
MH  - *Nanotubes, Carbon
MH  - *Pharmaceutical Preparations
MH  - Solid Phase Extraction
MH  - Spectroscopy, Fourier Transform Infrared
EDAT- 2018/10/27 06:00
MHDA- 2021/06/01 06:00
CRDT- 2018/10/27 06:00
PHST- 2018/10/27 06:00 [entrez]
PHST- 2018/10/27 06:00 [pubmed]
PHST- 2021/06/01 06:00 [medline]
AID - 10.1166/jnn.2019.15733 [doi]
PST - ppublish
SO  - J Nanosci Nanotechnol. 2019 Feb 1;19(2):627-633. doi: 10.1166/jnn.2019.15733.