PMID- 30477717
OWN - NLM
STAT- MEDLINE
DCOM- 20190215
LR  - 20190215
IS  - 1873-3778 (Electronic)
IS  - 0021-9673 (Linking)
VI  - 1584
DP  - 2019 Jan 11
TI  - MXene/reduced graphene oxide hydrogel film extraction combined with gas 
      chromatography-tandem mass spectrometry for the determination of 16 polycyclic 
      aromatic hydrocarbons in river and tap water.
PG  - 24-32
LID - S0021-9673(18)31436-5 [pii]
LID - 10.1016/j.chroma.2018.11.037 [doi]
AB  - In this study, MXene/reduced graphene oxide (MXene/rGO) hydrogel film, a novel 
      nanomaterial was prepared and used as adsorbent for extraction of 16 polycyclic 
      aromatic hydrocarbons (PAHs) in river and tap water prior to gas 
      chromatography-tandem mass spectrometric analysis (GC-MS/MS). The properties of 
      MXene/rGO hydrogel film were characterized by scanning electron microscope (SEM) 
      and X-ray diffractometer (XRD). The PAHs in water samples were enriched with 
      MXene/rGO, then eluted with n-hexane, finally separated with HP-5MS column 
      (30 m x 0.32 mm, 0.25 mum), and finally detected by mass spectrometer with SIM 
      mode. The method had linear ranges of 0.005-2.00 mug/L with the correlation 
      coefficients greater than 0.995. The recoveries of the method ranged from 80.3% 
      to 109.9%, with the relative standard deviations (RSDs) less than 10.01%. The 
      limits of detection (LODs) were less than 0.005 mug/L. The method is simple, 
      sensitive, precise, accurate, environmentally-friendly and it has been 
      successfully applied to the determination of 16 PAHs in river and tap water 
      samples.
CI  - Copyright (c) 2018 Elsevier B.V. All rights reserved.
FAU - Lingli, Qu
AU  - Lingli Q
AD  - West China School of Public Health, Sichuan University, Chengdu, 610041, China; 
      Putuo District Center for Disease Control and Prevention, Shanghai, 200333, 
      China.
FAU - Wang, Shengping
AU  - Wang S
AD  - School of Materials Science and Engineering, Tongji University, Shanghai, 201804, 
      China.
FAU - Yang, Xiaowei
AU  - Yang X
AD  - School of Materials Science and Engineering, Tongji University, Shanghai, 201804, 
      China.
FAU - Sun, Chengjun
AU  - Sun C
AD  - West China School of Public Health, Sichuan University, Chengdu, 610041, China. 
      Electronic address: sunchj@scu.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20181120
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Methylgalactosides)
RN  - 0 (Polycyclic Aromatic Hydrocarbons)
RN  - 0 (Water Pollutants, Chemical)
RN  - 0 (hydrogel film)
RN  - 059QF0KO0R (Water)
RN  - 7782-42-5 (Graphite)
SB  - IM
MH  - Gas Chromatography-Mass Spectrometry/*methods
MH  - Graphite/*chemistry
MH  - Limit of Detection
MH  - Methylgalactosides/*chemistry
MH  - Polycyclic Aromatic Hydrocarbons/*analysis/isolation & purification
MH  - Rivers/chemistry
MH  - Solid Phase Extraction/*methods
MH  - Tandem Mass Spectrometry/*methods
MH  - Water/chemistry
MH  - Water Pollutants, Chemical/*analysis/isolation & purification
OTO - NOTNLM
OT  - Gas chromatography-tandem mass spectrometry
OT  - MXene
OT  - Polycyclic aromatic hydrocarbons
OT  - Reduced graphene oxide
OT  - River water
OT  - Tap water
EDAT- 2018/11/28 06:00
MHDA- 2019/02/16 06:00
CRDT- 2018/11/28 06:00
PHST- 2018/08/17 00:00 [received]
PHST- 2018/10/29 00:00 [revised]
PHST- 2018/11/18 00:00 [accepted]
PHST- 2018/11/28 06:00 [pubmed]
PHST- 2019/02/16 06:00 [medline]
PHST- 2018/11/28 06:00 [entrez]
AID - S0021-9673(18)31436-5 [pii]
AID - 10.1016/j.chroma.2018.11.037 [doi]
PST - ppublish
SO  - J Chromatogr A. 2019 Jan 11;1584:24-32. doi: 10.1016/j.chroma.2018.11.037. Epub 
      2018 Nov 20.