PMID- 30574704
OWN - NLM
STAT- MEDLINE
DCOM- 20190103
LR  - 20190103
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 36
IP  - 12
DP  - 2018 Dec 8
TI  - [Determination of 39 veterinary drug residues in Procambarusclarkii by ultra-high 
      performance liquid chromatography-quadrupole-time of flight mass spectrometry].
PG  - 1261-1268
LID - 10.3724/SP.J.1123.2018.08037 [doi]
AB  - An ultra-high performance liquid chromatography-quadrupole time-of-flight mass 
      spectrometry (UHPLC-Q-TOF-MS) method was developed for determination of 39 
      veterinary drugs in Procambarusclarkii. Samples were extracted with acidified 
      acetonitrile and purified with enhanced matrix removal-lipid (EMR-Lipid) 
      adsorbent and graphitized multi-walled carbon nanotubes (GMWNTs). Extracts were 
      analyzed by UHPLC-Q-TOF-MS. Target compounds were screened according to accurate 
      mass, isotopic ratio, and retention time, and confirmed by library search. Target 
      analytes were quantified using the chromatographic peak area of each compound. 
      For each of the drugs of interest, calibration curves were linear in their 
      respective ranges with correlation coefficients greater than 0.99. The limits of 
      quantification (LOQs) were 3-15 mug/kg. The recoveries for target compounds spiked 
      in Procambarusclarkii ranged from 62.4% to 105.8%, with relative standard 
      deviations (RSDs) ranging from 2.5% to 13.5%. This method is simple, rapid, 
      accurate, and suitable for simultaneous determination of 39 veterinary drugs, 
      including sulfonamides, quinolones, and triphenylmethane, extracted from 
      Procambarusclarkii.
FAU - Song, Wei
AU  - Song W
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
AD  - Anhui Province Key Laboratory of Analysis and Detection for Food Safety, Hefei 
      230022, China.
FAU - Zhao, Muyu
AU  - Zhao M
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
FAU - Han, Fang
AU  - Han F
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
AD  - Anhui Province Key Laboratory of Analysis and Detection for Food Safety, Hefei 
      230022, China.
FAU - Lu, Yaning
AU  - Lu Y
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
AD  - Anhui Province Key Laboratory of Analysis and Detection for Food Safety, Hefei 
      230022, China.
FAU - Ding, Lei
AU  - Ding L
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
FAU - Zhou, Dianbing
AU  - Zhou D
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
FAU - Deng, Xiaojun
AU  - Deng X
AD  - Technical Center for Animal Plant and Food Inspection and Quarantine, Shanghai 
      Entry-Exit Inspection and Quarantine Bureau, Shanghai 200135, China.
FAU - Hu, Yanyun
AU  - Hu Y
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
AD  - Anhui Province Key Laboratory of Analysis and Detection for Food Safety, Hefei 
      230022, China.
FAU - Zheng, Ping
AU  - Zheng P
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
AD  - Anhui Province Key Laboratory of Analysis and Detection for Food Safety, Hefei 
      230022, China.
FAU - Sheng, Xuan
AU  - Sheng X
AD  - Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and 
      Quarantine Bureau, Hefei 230022 China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Nanotubes, Carbon)
RN  - 0 (Quinolones)
RN  - 0 (Sulfonamides)
RN  - 0 (Trityl Compounds)
RN  - 0 (Veterinary Drugs)
RN  - 8O4UTW9E17 (triphenylmethane)
SB  - IM
MH  - Animals
MH  - Astacoidea/*chemistry
MH  - *Chromatography, High Pressure Liquid
MH  - Drug Residues/*analysis
MH  - *Mass Spectrometry
MH  - Nanotubes, Carbon
MH  - Quinolones/analysis
MH  - Sulfonamides/analysis
MH  - Trityl Compounds/analysis
MH  - Veterinary Drugs/*analysis
OTO - NOTNLM
OT  - Procambarusclarkii
OT  - enhanced matrix removal-lipid adsorbent
OT  - graphitized multi-walled carbon nanotubes (GMWNTs)
OT  - ultra-high performance liquid chromatography-quadrupole-time of flight mass 
      spectrometry (UHPLC-Q-TOF-MS)
OT  - veterinary drug residues
EDAT- 2018/12/24 06:00
MHDA- 2019/01/04 06:00
CRDT- 2018/12/22 06:00
PHST- 2018/12/22 06:00 [entrez]
PHST- 2018/12/24 06:00 [pubmed]
PHST- 2019/01/04 06:00 [medline]
AID - 10.3724/SP.J.1123.2018.08037 [doi]
PST - ppublish
SO  - Se Pu. 2018 Dec 8;36(12):1261-1268. doi: 10.3724/SP.J.1123.2018.08037.