PMID- 30574713
OWN - NLM
STAT- MEDLINE
DCOM- 20190103
LR  - 20190103
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 36
IP  - 12
DP  - 2018 Dec 8
TI  - [Simultaneous determination of nine mycotoxins in cereal and cereal products by 
      high performance liquid chromatography with composite immunoaffinity clean-up 
      column].
PG  - 1330-1336
LID - 10.3724/SP.J.1123.2018.08008 [doi]
AB  - A rapid analytical method using high performance liquid chromatography (HPLC) 
      with post-column derivatization was established for the simultaneous 
      determination of nine mycotoxins in cereal and cereal products. The nine 
      mycotoxins were extracted from the samples by using acetone-water (80:20, v/v). 
      The extract was purified by a self-made composite immunoaffinity clean-up column 
      and was analyzed by HPLC. Mycotoxins were detected by fluorescence detection 
      after on-line photochemical derivatization and were quantified by an external 
      standard method. The nine compounds showed good linearities in their 
      concentration ranges with the correlation coefficients (R(2)) exceeding 0.999. 
      The spiked recoveries in real samples for the nine mycotoxins were above 80%, 
      while the relative standard deviations (RSDs) were in the range of 1.0%-5.6%. The 
      limits of detection (LODs) and the limits of quantification (LOQs) were 0.02-5.00 
      and 0.07-16.70 mug/kg, respectively. The developed method is simple, sensitive, 
      and has good repeatability, and thus can be used for the routine analysis of the 
      nine mycotoxins in cereal and cereal products.
FAU - Wang, Weigang
AU  - Wang W
AD  - Zhenjiang Center for Products Quality Supervision and Inspection, Zhenjiang 
      212132, China.
FAU - Qiang, Min
AU  - Qiang M
AD  - Zhenjiang Center for Products Quality Supervision and Inspection, Zhenjiang 
      212132, China.
FAU - Duan, Liqin
AU  - Duan L
AD  - Xuzhou Quality Inspection and Testing Center for Agricultural Products, Xuzhou 
      221006, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Mycotoxins)
SB  - IM
MH  - *Chromatography, High Pressure Liquid
MH  - Edible Grain/*chemistry
MH  - Fluorescence
MH  - *Food Contamination
MH  - Limit of Detection
MH  - Mycotoxins/*analysis
OTO - NOTNLM
OT  - cereal and cereal products
OT  - composite immunoaffinity column
OT  - high performance liquid chromatography (HPLC)
OT  - mycotoxin
EDAT- 2018/12/24 06:00
MHDA- 2019/01/04 06:00
CRDT- 2018/12/22 06:00
PHST- 2018/12/22 06:00 [entrez]
PHST- 2018/12/24 06:00 [pubmed]
PHST- 2019/01/04 06:00 [medline]
AID - 10.3724/SP.J.1123.2018.08008 [doi]
PST - ppublish
SO  - Se Pu. 2018 Dec 8;36(12):1330-1336. doi: 10.3724/SP.J.1123.2018.08008.