PMID- 30693707
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20190129
LR  - 20190129
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 37
IP  - 1
DP  - 2019 Jan 8
TI  - [Determination of 10 perfluorinated carboxylic acid compounds in water by gas 
      chromatography-mass spectrometry coupled with negative chemical ionization].
PG  - 32-39
LID - 10.3724/SP.J.1123.2018.07019 [doi]
AB  - A method was developed for the simultaneous determination of 10 perfluorinated 
      carboxylic acid compounds in water by gas chromatography-mass spectrometry 
      coupled with negative chemical ionization (GC-NCI-MS). Perfluorinated carboxylic 
      acid compounds were derivatized by trifluoro-N-methyl-N-(trimethylsilyl) 
      acetamide (MSTFA) as the trimethylsilyl derivatization reagent. The water sample 
      was purified and enriched through a weak anion exchange solid phase extraction 
      column and analyzed via GC-NCI-MS. The sample pretreatment, derivation and 
      instrument conditions were optimized. The results showed that the linearity of 
      the 10 perfluorinated carboxylic acid compounds was good in the range of 0.1-10 
      mg/L with correlation coefficients of 0.9956-0.9993. The limits of detection 
      (LODs) and limits of quantification (LOQs) were 0.5-1.5 mug/L and 1.5-4.5 mug/L, 
      respectively. The spiked recoveries of the blank samples ranged from 70.2% to 
      112.6% with the relative standard deviations (RSDs) between 2.1% and 14.5% (n=6). 
      The method is simple, sensitive, accurate and precise, and can be used to detect 
      the 10 perfluorinated carboxylic acid compounds in water.
FAU - Wang, Xiaoyan
AU  - Wang X
AD  - College of Pharmacy, Chian Pharmaceutical University, Nanjing 210009, China.
FAU - Shen, Weijian
AU  - Shen W
AD  - Animal, Plant and Food Inspection Center, Nanjing Customs, Nanjing 210009, China.
FAU - Wang, Hong
AU  - Wang H
AD  - Animal, Plant and Food Inspection Center, Nanjing Customs, Nanjing 210009, China.
FAU - Yu, Keyao
AU  - Yu K
AD  - Animal, Plant and Food Inspection Center, Nanjing Customs, Nanjing 210009, China.
FAU - Wu, Bin
AU  - Wu B
AD  - Animal, Plant and Food Inspection Center, Nanjing Customs, Nanjing 210009, China.
FAU - Hu, Guoshen
AU  - Hu G
AD  - Animal, Plant and Food Inspection Center, Nanjing Customs, Nanjing 210009, China.
FAU - Yang, Gongjun
AU  - Yang G
AD  - College of Pharmacy, Chian Pharmaceutical University, Nanjing 210009, China.
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
OTO - NOTNLM
OT  - gas chromatography-mass spectrometry (GC-MS)
OT  - negative chemical ionization (NCI)
OT  - perfluorinated carboxylic acid compounds
OT  - solid phase extraction (SPE)
OT  - water
EDAT- 2019/01/30 06:00
MHDA- 2019/01/30 06:01
CRDT- 2019/01/30 06:00
PHST- 2019/01/30 06:00 [entrez]
PHST- 2019/01/30 06:00 [pubmed]
PHST- 2019/01/30 06:01 [medline]
AID - 10.3724/SP.J.1123.2018.07019 [doi]
PST - ppublish
SO  - Se Pu. 2019 Jan 8;37(1):32-39. doi: 10.3724/SP.J.1123.2018.07019.