PMID- 30693709
OWN - NLM
STAT- MEDLINE
DCOM- 20190212
LR  - 20190215
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 37
IP  - 1
DP  - 2019 Jan 8
TI  - [Determination of 50 antibiotic residues in drone pupa powder by liquid 
      chromatography-tandem mass spectrometry].
PG  - 46-53
LID - 10.3724/SP.J.1123.2018.08046 [doi]
AB  - A method was established for the determination of 50 kinds of antibiotic residues 
      (macrolides, quinolones, sulfonamides, tetracyclines, nitroimidazoles, lincomycin 
      and chloramphenicol) in drone pupa powder by liquid chromatography-tandem mass 
      spectrometry (LC-MS/MS). The samples were extracted with perchloric acid and lead 
      acetate solution, and the protein was precipitated. The extraction solution was 
      adjusted to pH 8 using dipotassium hydrogen phosphate, then the solution was 
      purified by solid phase extraction (SPE) and analyzed by LC-MS/MS. The target 
      compounds in the drone pupa powder were determined quantitatively and 
      quantitatively by using multiple reaction monitoring and positive ion or negative 
      ion modes. The recoveries of the 50 antibiotics were in the range of 
      70.2%-118.3%, and the relative standard deviations (RSDs) were 1.8%-13.6%. The 
      method is simple, selective, and can be suitable for the analysis and 
      confirmation of veterinary drug residues in drone pupa powder.
FAU - Yang, Wenquan
AU  - Yang W
AD  - Animal, Plant and Food Inspection Center, Nanjing Customs, Nanjing 210001, China.
FAU - Zhang, Xiaoyan
AU  - Zhang X
AD  - Animal, Plant and Food Inspection Center, Nanjing Customs, Nanjing 210001, China.
FAU - Yao, Qian
AU  - Yao Q
AD  - Animal, Plant and Food Inspection Center, Nanjing Customs, Nanjing 210001, China.
FAU - Zhou, Yangjuan
AU  - Zhou Y
AD  - Southeast University Chengxian College, Nanjing 210088, China.
FAU - Hu, Yawen
AU  - Hu Y
AD  - Southeast University Chengxian College, Nanjing 210088, China.
FAU - Wang, Maohua
AU  - Wang M
AD  - China Certification & Accreditation Institute, Beijing 100020, China.
FAU - Tang, Maozhi
AU  - Tang M
AD  - China Certification & Accreditation Institute, Beijing 100020, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Anti-Bacterial Agents)
RN  - 0 (Veterinary Drugs)
SB  - IM
MH  - Animals
MH  - Anti-Bacterial Agents/*analysis
MH  - Chromatography, Liquid
MH  - Drug Residues/*analysis
MH  - Pupa/*chemistry
MH  - Solid Phase Extraction
MH  - Tandem Mass Spectrometry
MH  - Veterinary Drugs/*analysis
OTO - NOTNLM
OT  - antibiotic residues
OT  - drone pupa powder
OT  - liquid chromatography-tandem mass spectrometry (LC-MS/MS)
OT  - solid phase extraction (SPE)
EDAT- 2019/01/30 06:00
MHDA- 2019/02/13 06:00
CRDT- 2019/01/30 06:00
PHST- 2019/01/30 06:00 [entrez]
PHST- 2019/01/30 06:00 [pubmed]
PHST- 2019/02/13 06:00 [medline]
AID - 10.3724/SP.J.1123.2018.08046 [doi]
PST - ppublish
SO  - Se Pu. 2019 Jan 8;37(1):46-53. doi: 10.3724/SP.J.1123.2018.08046.