PMID- 30724249
OWN - NLM
STAT- MEDLINE
DCOM- 20190319
LR  - 20190319
IS  - 1873-7072 (Electronic)
IS  - 0308-8146 (Linking)
VI  - 275
DP  - 2019 Mar 1
TI  - In vivo analysis of two new fungicides in mung bean sprouts by solid phase 
      microextraction-gas chromatography-mass spectrometry.
PG  - 688-695
LID - S0308-8146(18)31726-6 [pii]
LID - 10.1016/j.foodchem.2018.09.148 [doi]
AB  - A novel solid phase microextraction-gas chromatography-mass spectrometry 
      (SPME-GC-MS) method was developed to quantify two new fungicide residuals 
      (Y13149, Y12196) in mung bean sprouts. With a stable and biocompatible 
      elcetrospinning nanofiber (polystyrene/graphene@silica, PS/G@SiO(2)) as coating, 
      the SPME fiber was directly inserted into the stem of mung bean sprout to in-situ 
      in-vivo sampling and extraction, followed by GC-MS analysis. Under the optimal 
      conditions, satisfactory average recoveries of 99% and 72% were obtained for 
      Y13149 and Y12196 with the relative standard deviations (RSDs) under 16.3%, 
      indicating good precision and anti-matrix ability of the method. The result also 
      exhibited low detection limit (0.06-0.08 mug.L(-1)) and wide liner range 
      (0.3-100 mug.L(-1)) with the correlation coefficients (R(2)) of 0.9989. The 
      established method was applied successfully to trace the accumulation and 
      distribution of fungicides in mung bean sprouts, and it provides a simple, rapid 
      and reliable quantitative method for food analysis.
CI  - Copyright (c) 2018 Elsevier Ltd. All rights reserved.
FAU - Shi, Zhen
AU  - Shi Z
AD  - Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of 
      Chemistry, Central China Normal University, Wuhan, China.
FAU - Chen, Dan
AU  - Chen D
AD  - Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of 
      Chemistry, Central China Normal University, Wuhan, China.
FAU - Chen, Tian-Tian
AU  - Chen TT
AD  - Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of 
      Chemistry, Central China Normal University, Wuhan, China.
FAU - Wei, Ge
AU  - Wei G
AD  - Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of 
      Chemistry, Central China Normal University, Wuhan, China.
FAU - Yin, Chun-Yan
AU  - Yin CY
AD  - Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of 
      Chemistry, Central China Normal University, Wuhan, China.
FAU - Xu, Hui
AU  - Xu H
AD  - Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of 
      Chemistry, Central China Normal University, Wuhan, China. Electronic address: 
      huixu@mail.ccnu.edu.cn.
FAU - Yang, Guang-Fu
AU  - Yang GF
AD  - Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of 
      Chemistry, Central China Normal University, Wuhan, China. Electronic address: 
      gfyang@mail.ccnu.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20180925
PL  - England
TA  - Food Chem
JT  - Food chemistry
JID - 7702639
RN  - 0 (Fungicides, Industrial)
RN  - 0 (Polystyrenes)
RN  - 7631-86-9 (Silicon Dioxide)
RN  - 7782-42-5 (Graphite)
SB  - IM
MH  - Food Analysis
MH  - Fungicides, Industrial/*analysis/isolation & purification
MH  - Gas Chromatography-Mass Spectrometry/*methods
MH  - Graphite/chemistry
MH  - Limit of Detection
MH  - Nanofibers/chemistry
MH  - Polystyrenes/chemistry
MH  - Silicon Dioxide/chemistry
MH  - Solid Phase Microextraction
MH  - Vigna/*chemistry/metabolism
OTO - NOTNLM
OT  - Fungicides
OT  - Gas chromatography-mass spectrometry
OT  - In vivo
OT  - Mung bean sprouts
OT  - Polystyrene/graphene@silica
OT  - Solid phase microextraction
EDAT- 2019/02/07 06:00
MHDA- 2019/03/20 06:00
CRDT- 2019/02/07 06:00
PHST- 2018/07/05 00:00 [received]
PHST- 2018/09/15 00:00 [revised]
PHST- 2018/09/24 00:00 [accepted]
PHST- 2019/02/07 06:00 [entrez]
PHST- 2019/02/07 06:00 [pubmed]
PHST- 2019/03/20 06:00 [medline]
AID - S0308-8146(18)31726-6 [pii]
AID - 10.1016/j.foodchem.2018.09.148 [doi]
PST - ppublish
SO  - Food Chem. 2019 Mar 1;275:688-695. doi: 10.1016/j.foodchem.2018.09.148. Epub 2018 
      Sep 25.