PMID- 31108803
OWN - NLM
STAT- MEDLINE
DCOM- 20200921
LR  - 20200921
IS  - 1873-7145 (Electronic)
IS  - 0963-9969 (Linking)
VI  - 121
DP  - 2019 Jul
TI  - HS-SPME-GC-MS technique for FFA and hexanal analysis in different cheese 
      packaging in the course of long term storage.
PG  - 730-737
LID - S0963-9969(18)30995-5 [pii]
LID - 10.1016/j.foodres.2018.12.048 [doi]
AB  - The present study sought to develop a headspace solid-phase microextraction 
      (HS-SPME) gas chromatography-mass spectrometry (GC-MS) method to quantify free 
      fatty acids (FFAs) and hexanal in cheese, and to track theirs levels over time. 
      The developed method was applied on Fresh Asiago and Grana Padano cheeses, and 
      FFAs and hexanal levels were monitored over 4 and 12 weeks respectively. Their 
      evolutions were also compared from two types of packaging films: a high-density 
      polyethylene (HDPE) package and a packaging bag named Ideabrill(R). The later 
      allowed a lower increase of these analytes (11.6-fold increase for Grana Padano 
      and 5.9 for Fresh Asiago) compared to the HDPE packaging (21.5-fold increase for 
      Grana Padano and 7.4 for Fresh Asiago). This method can contribute to the 
      optimization of analytical methods in food industry for studies on shelf life, 
      quality control or food packaging.
CI  - Copyright (c) 2018 Elsevier Ltd. All rights reserved.
FAU - Nzekoue, Franks Kamgang
AU  - Nzekoue FK
AD  - School of Pharmacy, University of Camerino, Via Sant'Agostino 1, Camerino 62032, 
      Italy.
FAU - Caprioli, Giovanni
AU  - Caprioli G
AD  - School of Pharmacy, University of Camerino, Via Sant'Agostino 1, Camerino 62032, 
      Italy. Electronic address: giovanni.caprioli@unicam.it.
FAU - Fiorini, Dennis
AU  - Fiorini D
AD  - School of Science and Technology, Chemistry Division, University of Camerino, Via 
      S. Agostino 1, Camerino 62032, Italy.
FAU - Torregiani, Elisabetta
AU  - Torregiani E
AD  - School of Pharmacy, University of Camerino, Via Sant'Agostino 1, Camerino 62032, 
      Italy.
FAU - Vittori, Sauro
AU  - Vittori S
AD  - School of Pharmacy, University of Camerino, Via Sant'Agostino 1, Camerino 62032, 
      Italy.
FAU - Sagratini, Gianni
AU  - Sagratini G
AD  - School of Pharmacy, University of Camerino, Via Sant'Agostino 1, Camerino 62032, 
      Italy.
LA  - eng
PT  - Journal Article
DEP - 20181224
PL  - Canada
TA  - Food Res Int
JT  - Food research international (Ottawa, Ont.)
JID - 9210143
RN  - 0 (Aldehydes)
RN  - 0 (Fatty Acids, Nonesterified)
RN  - 0 (Volatile Organic Compounds)
RN  - 9DC2K31JJQ (n-hexanal)
SB  - IM
MH  - Aldehydes/*analysis
MH  - Cheese/*analysis
MH  - Fatty Acids, Nonesterified/*analysis
MH  - Food Analysis
MH  - Food Packaging
MH  - *Food Storage
MH  - *Gas Chromatography-Mass Spectrometry
MH  - *Solid Phase Microextraction
MH  - Volatile Organic Compounds/analysis
OTO - NOTNLM
OT  - 2-methylpentanal (PubChem: CID 31245)
OT  - Cheese
OT  - Food packaging
OT  - Free fatty acids
OT  - HS-SPME-GC-MS
OT  - Hexanal
OT  - Hexanal (PubChem: CID 6184)
OT  - Octanoic acid (PubChem: CID 379)
OT  - Shelf life
OT  - butanoic acid (PubChem: CID 71308900)
OT  - decanoic acid (PubChem: CID 12209363)
OT  - hexanoic acid (PubChem: CID 12222600)
OT  - isovaleric acid (PubChem: CID 10430)
EDAT- 2019/05/22 06:00
MHDA- 2020/09/22 06:00
CRDT- 2019/05/22 06:00
PHST- 2018/09/19 00:00 [received]
PHST- 2018/12/17 00:00 [revised]
PHST- 2018/12/22 00:00 [accepted]
PHST- 2019/05/22 06:00 [entrez]
PHST- 2019/05/22 06:00 [pubmed]
PHST- 2020/09/22 06:00 [medline]
AID - S0963-9969(18)30995-5 [pii]
AID - 10.1016/j.foodres.2018.12.048 [doi]
PST - ppublish
SO  - Food Res Int. 2019 Jul;121:730-737. doi: 10.1016/j.foodres.2018.12.048. Epub 2018 
      Dec 24.