PMID- 31122443 OWN - NLM STAT- MEDLINE DCOM- 20190617 LR - 20190617 IS - 1873-3573 (Electronic) IS - 0039-9140 (Linking) VI - 201 DP - 2019 Aug 15 TI - Covalent immobilization of covalent organic framework on stainless steel wire for solid-phase microextraction GC-MS/MS determination of sixteen polycyclic aromatic hydrocarbons in grilled meat samples. PG - 413-418 LID - S0039-9140(19)30420-5 [pii] LID - 10.1016/j.talanta.2019.04.031 [doi] AB - Covalent organic framework TpBD was grafted on stainless steel wire with polydopamine as a linker. The fabricated TpBD bonded stainless steel wire was used as the solid-phase microextraction fiber to extract sixteen polycyclic aromatic hydrocarbons (PAHs) for subsequent GC-MS/MS determination in grilled meat samples. The developed method gave the limits of detection (S/N = 3) from 0.02 (pyrene)-1.66 (naphthalene) ng L(-1) and enhancement factors from 1069 (naphthalene)-10879 (benz(a)anthracene). The relative standard deviations (RSDs) for intra-day and inter-day study are in the range of 2.6%-8.5% and 4.5%-9.4%, respectively. The fiber-to-fiber RSDs for three parallel prepared fibers were 5.3%-10.0%. One TpBD bonded fiber can stand at least 200 cycles without significant loss of extraction efficiency. The developed method was successfully applied for the determination of trace PAHs in grilled meat samples with recoveries from 85.1% to 102.8%. CI - Copyright (c) 2019 Elsevier B.V. All rights reserved. FAU - Ma, Tian-Tian AU - Ma TT AD - State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi, 214122, China; Institute of Analytical Food Safety, School of Food Science and Technology, Jiangnan University, Wuxi, 214122, China. FAU - Shen, Xiao-Fang AU - Shen XF AD - State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi, 214122, China; Institute of Analytical Food Safety, School of Food Science and Technology, Jiangnan University, Wuxi, 214122, China. FAU - Yang, Cheng AU - Yang C AD - State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi, 214122, China; Institute of Analytical Food Safety, School of Food Science and Technology, Jiangnan University, Wuxi, 214122, China. FAU - Qian, Hai-Long AU - Qian HL AD - State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi, 214122, China; Institute of Analytical Food Safety, School of Food Science and Technology, Jiangnan University, Wuxi, 214122, China. FAU - Pang, Yue-Hong AU - Pang YH AD - State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi, 214122, China; Institute of Analytical Food Safety, School of Food Science and Technology, Jiangnan University, Wuxi, 214122, China. Electronic address: yhpang@jiangnan.edu.cn. FAU - Yan, Xiu-Ping AU - Yan XP AD - State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi, 214122, China; Institute of Analytical Food Safety, School of Food Science and Technology, Jiangnan University, Wuxi, 214122, China; Key Laboratory of Synthetic and Biological Colloids, Ministry of Education, Jiangnan University, Wuxi, 214122, China. Electronic address: xpyan@jiangnan.edu.cn. LA - eng PT - Journal Article DEP - 20190412 PL - Netherlands TA - Talanta JT - Talanta JID - 2984816R RN - 0 (Indoles) RN - 0 (Metal-Organic Frameworks) RN - 0 (Polycyclic Aromatic Hydrocarbons) RN - 0 (Polymers) RN - 0 (polydopamine) RN - 12597-68-1 (Stainless Steel) SB - IM MH - Animals MH - Chickens MH - Food Contamination/*analysis MH - Gas Chromatography-Mass Spectrometry/methods MH - Indoles/chemistry MH - Limit of Detection MH - Meat/*analysis MH - Metal-Organic Frameworks/*chemistry MH - Polycyclic Aromatic Hydrocarbons/*analysis MH - Polymers/chemistry MH - Poultry Products/analysis MH - Red Meat/analysis MH - Sheep MH - Solid Phase Microextraction/instrumentation/*methods MH - Stainless Steel/*chemistry MH - Swine MH - Tandem Mass Spectrometry/methods OTO - NOTNLM OT - Covalent organic frameworks OT - GC-MS OT - Grilled meat OT - Polycyclic aromatic hydrocarbons OT - Solid-phase microextraction EDAT- 2019/05/28 06:00 MHDA- 2019/06/18 06:00 CRDT- 2019/05/25 06:00 PHST- 2019/03/04 00:00 [received] PHST- 2019/04/09 00:00 [revised] PHST- 2019/04/11 00:00 [accepted] PHST- 2019/05/25 06:00 [entrez] PHST- 2019/05/28 06:00 [pubmed] PHST- 2019/06/18 06:00 [medline] AID - S0039-9140(19)30420-5 [pii] AID - 10.1016/j.talanta.2019.04.031 [doi] PST - ppublish SO - Talanta. 2019 Aug 15;201:413-418. doi: 10.1016/j.talanta.2019.04.031. Epub 2019 Apr 12.