PMID- 31122445
OWN - NLM
STAT- MEDLINE
DCOM- 20190617
LR  - 20190617
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 201
DP  - 2019 Aug 15
TI  - Porous covalent triazine-terphenyl polymer as hydrophilic-lipophilic balanced 
      sorbent for solid phase extraction of tetracyclines in animal derived foods.
PG  - 426-432
LID - S0039-9140(19)30399-6 [pii]
LID - 10.1016/j.talanta.2019.04.010 [doi]
AB  - A novel hydrophilic-lipophilic balanced (HLB) solid phase extraction sorbent, 
      microporous covalent triazine-terphenyl polymer (CTP(CC-TP)) was successfully 
      synthesized and applied for the cleanup and extraction of tetracycline drugs in 
      animal derived food samples. The specific ratio of two monomers, hydrophilic 
      triazine and lipophilic aromatic rings, endowed the new material with 
      hydrophilic-lipophilic balanced character, which made it capable of extracting 
      both polar and nonpolar analytes. Prior to solid-phase extraction, food samples 
      were extracted by McIlvaine buffer and passed through the CTP(CC-TP) cartridge. 
      The experimental parameters affecting extraction efficiency, including loading, 
      washing and elution were investigated and optimized. With the use of 
      high-performance liquid chromatography-UV detection, a method detection limit in 
      the range of 8.0-16.8 mug kg(-1) and good linearity (22.6-1500 mug kg(-1)) for the 
      determination of the tetracyclines in animal derived food samples can be 
      achieved. The relative standard deviations (RSDs) for five replicate extractions 
      of the tetracyclines ranged from 4.8 to 8.2%. The method recoveries for spiked 
      tetracyclines (100 and 1000 mug kg(-1)) in bovine milk, egg, chicken liver samples 
      were in the range of 81.3-98.7% with RSDs ranging from 3.9 to 7.7%, respectively, 
      depending on both the analytes and samples. The method was suitable for the 
      determination of tetracyclines in animal derived food samples.
CI  - Copyright (c) 2019. Published by Elsevier B.V.
FAU - Zhao, Wenjie
AU  - Zhao W
AD  - College of Chemistry, Chemical and Environmental Engineering, Henan University of 
      Technology, Zhengzhou, 450001, PR China. Electronic address: wjiezh@126.com.
FAU - Zuo, Huiying
AU  - Zuo H
AD  - College of Chemistry, Chemical and Environmental Engineering, Henan University of 
      Technology, Zhengzhou, 450001, PR China.
FAU - Guo, Yun
AU  - Guo Y
AD  - College of Chemistry and Molecular Engineering, Key Laboratory of Chemical 
      Biology and Organic Chemistry of Henan, Zhengzhou University, Zhengzhou, 450001, 
      PR China.
FAU - Liu, Kejian
AU  - Liu K
AD  - Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou, 450008, PR China.
FAU - Wang, Sheng
AU  - Wang S
AD  - Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou, 450008, PR China.
FAU - He, Lijun
AU  - He L
AD  - College of Chemistry, Chemical and Environmental Engineering, Henan University of 
      Technology, Zhengzhou, 450001, PR China.
FAU - Jiang, Xiuming
AU  - Jiang X
AD  - College of Chemistry, Chemical and Environmental Engineering, Henan University of 
      Technology, Zhengzhou, 450001, PR China.
FAU - Xiang, Guoqiang
AU  - Xiang G
AD  - College of Chemistry, Chemical and Environmental Engineering, Henan University of 
      Technology, Zhengzhou, 450001, PR China.
FAU - Zhang, Shusheng
AU  - Zhang S
AD  - College of Chemistry and Molecular Engineering, Key Laboratory of Chemical 
      Biology and Organic Chemistry of Henan, Zhengzhou University, Zhengzhou, 450001, 
      PR China. Electronic address: zsszz@126.com.
LA  - eng
PT  - Journal Article
DEP - 20190409
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
RN  - 0 (Anti-Bacterial Agents)
RN  - 0 (Polymers)
RN  - 0 (Terphenyl Compounds)
RN  - 0 (Tetracyclines)
RN  - 0 (Triazines)
SB  - IM
MH  - Adsorption
MH  - Animals
MH  - Anti-Bacterial Agents/*analysis
MH  - Cattle
MH  - Chickens
MH  - Chromatography, High Pressure Liquid/methods
MH  - Eggs/analysis
MH  - Food Contamination/*analysis
MH  - Hydrophobic and Hydrophilic Interactions
MH  - Limit of Detection
MH  - Liver/chemistry
MH  - Milk/chemistry
MH  - Polymers/*chemistry
MH  - Porosity
MH  - Poultry Products/analysis
MH  - Solid Phase Extraction/methods
MH  - Terphenyl Compounds/*chemistry
MH  - Tetracyclines/*analysis
MH  - Triazines/*chemistry
OTO - NOTNLM
OT  - Animal derived foods
OT  - Covalent triazine polymer
OT  - Hydrophilic-lipophilic balance
OT  - Solid phase extraction
OT  - Tetracyclines
EDAT- 2019/05/28 06:00
MHDA- 2019/06/18 06:00
CRDT- 2019/05/25 06:00
PHST- 2018/11/22 00:00 [received]
PHST- 2019/03/12 00:00 [revised]
PHST- 2019/04/04 00:00 [accepted]
PHST- 2019/05/25 06:00 [entrez]
PHST- 2019/05/28 06:00 [pubmed]
PHST- 2019/06/18 06:00 [medline]
AID - S0039-9140(19)30399-6 [pii]
AID - 10.1016/j.talanta.2019.04.010 [doi]
PST - ppublish
SO  - Talanta. 2019 Aug 15;201:426-432. doi: 10.1016/j.talanta.2019.04.010. Epub 2019 
      Apr 9.