PMID- 31642281
OWN - NLM
STAT- MEDLINE
DCOM- 20191025
LR  - 20200108
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 37
IP  - 10
DP  - 2019 Oct 8
TI  - [Determination of pesticide residues in wolfberry using QuEChERS-gas 
      chromatography-tandem mass spectrometry].
PG  - 1042-1047
LID - 10.3724/SP.J.1123.2019.04014 [doi]
AB  - A method based on QuEChERS-gas chromatography-tandem mass spectrometry (GC-MS/MS) 
      was established for the determination of 20 pesticide residues in wolfberry. The 
      samples were extracted with acetonitrile. The extract was purified with PSA 
      (primary secondary amine), GCB (graphite carbon black) and C(18) to suppress the 
      matrix in wolfberry. The analytical results showed that the calibration curves 
      for the 20 pesticides obtained by GC-MS/MS were linear in the range of 5-500 
      mug/L, with the correlation coefficients higher than 0.99. The recoveries ranged 
      from 70.02% to 110.78% with relative standard deviations (RSDs) ranging from 
      2.05% to 9.53%. This method has the advantages of being time-saving, convenient 
      and sensitive. The proposed method can simultaneously detect organic phosphorus 
      and organic chlorine pesticides residues with a good performance in terms of 
      qualitative and quantitative detection.
FAU - Wang, Fanghuan
AU  - Wang F
AD  - Yinchuan Customs Integrated Technology Center, Yinchuan 750002, China.
FAU - Ren, Cuijuan
AU  - Ren C
AD  - Yinchuan Customs Integrated Technology Center, Yinchuan 750002, China.
FAU - Ma, Hui
AU  - Ma H
AD  - Yinchuan Customs Integrated Technology Center, Yinchuan 750002, China.
FAU - Li, Ping
AU  - Li P
AD  - Yinchuan Customs Integrated Technology Center, Yinchuan 750002, China.
FAU - Hao, Junhu
AU  - Hao J
AD  - Yinchuan Customs Integrated Technology Center, Yinchuan 750002, China.
FAU - Chen, Lin
AU  - Chen L
AD  - Yinchuan Customs Integrated Technology Center, Yinchuan 750002, China.
FAU - Sun, Min
AU  - Sun M
AD  - Yinchuan Customs Integrated Technology Center, Yinchuan 750002, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Pesticide Residues)
SB  - IM
MH  - Gas Chromatography-Mass Spectrometry
MH  - Lycium/*chemistry
MH  - Pesticide Residues/*analysis
MH  - Tandem Mass Spectrometry
OTO - NOTNLM
OT  - QuEChERS
OT  - gas-chromatography-tandem mass spectrometry (GC-MS/MS)
OT  - pesticide residues
OT  - wolfberry
EDAT- 2019/10/24 06:00
MHDA- 2019/10/28 06:00
CRDT- 2019/10/24 06:00
PHST- 2019/10/24 06:00 [entrez]
PHST- 2019/10/24 06:00 [pubmed]
PHST- 2019/10/28 06:00 [medline]
AID - 10.3724/SP.J.1123.2019.04014 [doi]
PST - ppublish
SO  - Se Pu. 2019 Oct 8;37(10):1042-1047. doi: 10.3724/SP.J.1123.2019.04014.