PMID- 31642290
OWN - NLM
STAT- MEDLINE
DCOM- 20191025
LR  - 20240109
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 37
IP  - 10
DP  - 2019 Oct 8
TI  - [Rapid simultaneous determination of 10 nutrients in ginger by ultra-high 
      performance liquid chromatography-tandem mass spectrometry].
PG  - 1105-1111
LID - 10.3724/SP.J.1123.2019.03024 [doi]
AB  - An analytical method by ultra-high performance liquid chromatography-tandem mass 
      spectrometry (UHPLC-MS/MS) was developed for the simultaneous determination of 
      the two types of nutrients, viz. gingerol-related compounds and curcuminoids in 
      ginger, including 6-gingerol, 8-gingerol, 10-gingerol, 6-shogaol, 8-shogaol, 
      10-shogaol, tetrahydrocurcumin, curcumin, demethoxycurcumin and 
      bisdemethoxycurcumin. The 10 target compounds were separated on a ZORBAX RRHD 
      Eclipse Plus C18 column (100 mmx2.1 mm, 1.8 mum) using gradient elution with 0.1% 
      (v/v) formic acid aqueous solution and methanol containing 0.1% (v/v) formic acid 
      as the mobile phases. Qualitative confirmation and quantitative analysis of the 
      target compounds were performed using an electrospray ionization (ESI) source in 
      the positive ion and multiple reaction monitoring (MRM) modes. The linear 
      correlation coefficients (r) of the 10 nutrients were >/= 0.9995. The limits of 
      quantification were 0.10-7.71 mug/L. The average spiked recoveries of the samples 
      at the three levels were 82.8%-115.3%, the relative standard deviations (RSDs) 
      were 0.58%-11.49%. The results showed that all the 10 nutrients in ginger were 
      detected, and the content of 6-gingerol was the highest at 373.35-702.48 mg/kg. 
      This method is convenient, rapid, accurate and reliable, and is suitable for the 
      analysis of gingerol-related and curcuminoids in ginger. It provides a technical 
      means for the quality identification and control of ginger.
FAU - Zhang, Wenhuan
AU  - Zhang W
AD  - Institute of Quality Standard and Testing Technology for Agro-Products of Chinese 
      Academy of Agricultural Sciences, Key Laboratory of Agri-food Quality and Safety, 
      Ministry of Agriculture and Rural Affairs, Beijing 100081, China.
FAU - Liu, Pingxiang
AU  - Liu P
AD  - Institute of Quality Standard and Testing Technology for Agro-Products of Chinese 
      Academy of Agricultural Sciences, Key Laboratory of Agri-food Quality and Safety, 
      Ministry of Agriculture and Rural Affairs, Beijing 100081, China.
FAU - Qiu, Jing
AU  - Qiu J
AD  - Institute of Quality Standard and Testing Technology for Agro-Products of Chinese 
      Academy of Agricultural Sciences, Key Laboratory of Agri-food Quality and Safety, 
      Ministry of Agriculture and Rural Affairs, Beijing 100081, China.
FAU - Jia, Qi
AU  - Jia Q
AD  - Institute of Quality Standard and Testing Technology for Agro-Products of Chinese 
      Academy of Agricultural Sciences, Key Laboratory of Agri-food Quality and Safety, 
      Ministry of Agriculture and Rural Affairs, Beijing 100081, China.
FAU - Qian, Yongzhong
AU  - Qian Y
AD  - Institute of Quality Standard and Testing Technology for Agro-Products of Chinese 
      Academy of Agricultural Sciences, Key Laboratory of Agri-food Quality and Safety, 
      Ministry of Agriculture and Rural Affairs, Beijing 100081, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Phytochemicals)
SB  - IM
MH  - Chromatography, High Pressure Liquid
MH  - Food Analysis/*methods
MH  - Zingiber officinale/*chemistry
MH  - Nutrients/*analysis
MH  - Phytochemicals/*analysis
MH  - Tandem Mass Spectrometry
OTO - NOTNLM
OT  - curcumin
OT  - ginger
OT  - gingerol
OT  - nutrients
OT  - shogaol
OT  - ultra-high performance liquid chromatography-tandem mass spectrometry 
      (UHPLC-MS/MS)
EDAT- 2019/10/24 06:00
MHDA- 2019/10/28 06:00
CRDT- 2019/10/24 06:00
PHST- 2019/10/24 06:00 [entrez]
PHST- 2019/10/24 06:00 [pubmed]
PHST- 2019/10/28 06:00 [medline]
AID - 10.3724/SP.J.1123.2019.03024 [doi]
PST - ppublish
SO  - Se Pu. 2019 Oct 8;37(10):1105-1111. doi: 10.3724/SP.J.1123.2019.03024.