PMID- 31642291
OWN - NLM
STAT- MEDLINE
DCOM- 20191025
LR  - 20200108
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 37
IP  - 10
DP  - 2019 Oct 8
TI  - [Determination of benzimidazoles residue markers in chicken tissue by high 
      performance liquid chromatography].
PG  - 1112-1117
LID - 10.3724/SP.J.1123.2019.03031 [doi]
AB  - A method was developed for the simultaneous determination of 11 benzimildazoles 
      residue markers in chicken meat, liver and kidney samples by high performance 
      liquid chromatography (HPLC). The chicken tissue sample was extracted with 
      acetonitrile, defatted with n-hexane, and purified with an MCX solid-phase 
      extraction cartridge. Chromatographic separation was performed on an Atlantis 
      T(3) column with the gradient elution of methyl alcohol-1% (v/v) acetic acid 
      aqueous solution as the mobile phases at a flow rate of 1.0 mL/min. The detection 
      wavelength was set at 292 nm. Analytes were quantified by the external standard 
      method. The linearities of the calibration curves were well in the range of 
      25-1000 mug/L, and the limit of quantification was 50 mug/kg. The recoveries at 
      different spiked levels in all the three matrices ranged from 70.91% to 103.21%, 
      and the relative standard deviations (RSDs) were between 1.48% and 10.08% (n=6). 
      The developed method is characterized by an excellent purification effect, 
      sensitivity and accuracy, and can be used for the determination of benzimidazoles 
      residue markers in chicken tissue samples.
FAU - Zou, You
AU  - Zou Y
AD  - Guangdong Inspection and Quarantine Technology Center, Guangzhou 510623, China.
FAU - Shao, Linzhi
AU  - Shao L
AD  - Guangdong Inspection and Quarantine Technology Center, Guangzhou 510623, China.
FAU - Wu, Yingxuan
AU  - Wu Y
AD  - Guangdong Inspection and Quarantine Technology Center, Guangzhou 510623, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Benzimidazoles)
SB  - IM
MH  - Animals
MH  - Benzimidazoles/*analysis
MH  - Chickens
MH  - Chromatography, High Pressure Liquid
MH  - Food Contamination/*analysis
MH  - Meat/*analysis
MH  - Solid Phase Extraction
OTO - NOTNLM
OT  - benzimidazoles residue markers
OT  - chicken tissue
OT  - high performance liquid chromatography (HPLC)
OT  - solid phase extraction(SPE)
EDAT- 2019/10/24 06:00
MHDA- 2019/10/28 06:00
CRDT- 2019/10/24 06:00
PHST- 2019/10/24 06:00 [entrez]
PHST- 2019/10/24 06:00 [pubmed]
PHST- 2019/10/28 06:00 [medline]
AID - 10.3724/SP.J.1123.2019.03031 [doi]
PST - ppublish
SO  - Se Pu. 2019 Oct 8;37(10):1112-1117. doi: 10.3724/SP.J.1123.2019.03031.