PMID- 31642305
OWN - NLM
STAT- MEDLINE
DCOM- 20191025
LR  - 20200108
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 37
IP  - 9
DP  - 2019 Sep 8
TI  - [Simultaneous determination of twenty amino acids and six carbohydrates in soy 
      sauce by ion chromatography with integrated pulsed amperometric detection].
PG  - 996-1003
LID - 10.3724/SP.J.1123.2019.03030 [doi]
AB  - A method of gradient elution ion chromatography with integrated pulsed 
      amperometric detection for simultaneous determination of twenty amino acids and 
      six carbohydrates in soy sauce was established. The effects of column 
      temperature, pH value of solution, and standing time were studied, and then the 
      suitable gradient elution conditions were found for the determination. In the 
      conditions that the flow rate is 0.25 mL/min, pH value of solution is in the 
      range of 5.2-6.7, temperature of column is 35℃, the linear relationships of the 
      26 components are good and the correlation coefficients are not less than 0.995. 
      Except glutamine, leucine, isoleucine and methionine, the limits of detection 
      (S/N=3) of the other 22 components are less than 0.03 mg/L. The recoveries of the 
      26 components in soy sauce are 84.2%-109% at the spiked levels of 0.20, 0.50, 
      2.00 mg/L, and the relative standard deviations (RSDs) are in the range of 
      2.7%-7.8%. The method is efficient, easy, sensitive, and accurate for 
      simultaneous determination of amino acids and carbohydrates in soy sauce, and can 
      provide an effective research technique for adulterated soy sauce.
FAU - Song, Weide
AU  - Song W
AD  - Rizhao Customs, Rizhao 276826, China.
FAU - Su, Zheng
AU  - Su Z
AD  - Rizhao Customs, Rizhao 276826, China.
FAU - Hui, Xidong
AU  - Hui X
AD  - Rizhao Customs, Rizhao 276826, China.
FAU - Xu, Chonglong
AU  - Xu C
AD  - Rizhao Customs, Rizhao 276826, China.
FAU - Du, Lijun
AU  - Du L
AD  - Taiyuan Customs, Taiyuan 030024, China.
FAU - Zhang, Chuanjie
AU  - Zhang C
AD  - Rizhao Customs, Rizhao 276826, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Amino Acids)
RN  - 0 (Carbohydrates)
SB  - IM
MH  - Amino Acids/*analysis
MH  - Carbohydrates/*analysis
MH  - Chromatography, Ion Exchange
MH  - Soy Foods/*analysis
OTO - NOTNLM
OT  - amino acid
OT  - carbohydrate
OT  - gradient elution
OT  - integrated pulsed amperometric detection
OT  - ion chromatography (IC)
OT  - soy sauce
EDAT- 2019/10/24 06:00
MHDA- 2019/10/28 06:00
CRDT- 2019/10/24 06:00
PHST- 2019/10/24 06:00 [entrez]
PHST- 2019/10/24 06:00 [pubmed]
PHST- 2019/10/28 06:00 [medline]
AID - 10.3724/SP.J.1123.2019.03030 [doi]
PST - ppublish
SO  - Se Pu. 2019 Sep 8;37(9):996-1003. doi: 10.3724/SP.J.1123.2019.03030.