PMID- 31696162
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20200929
IS  - 2661-801X (Electronic)
IS  - 2661-801X (Linking)
VI  - 13
IP  - 1
DP  - 2019 Dec
TI  - Direct analysis of volatile components from intact jujube by carbon fiber 
      ionization mass spectrometry.
PG  - 125
LID - 10.1186/s13065-019-0641-4 [doi]
LID - 125
AB  - In situ analysis of odor is an important approach to connect odor with chemical 
      composition. However, it is difficult to conduct a rapid direct analysis of the 
      odor sample because of low analyte concentration and sampling. To achieve the 
      direct analysis, a carbon fiber ionization mass spectrometry (CFI-MS) method has 
      been developed and applied to measure volatile components releasing from intact 
      jujube. To build the CFI source, a 2.0-cm long carbon fiber bundle was integrated 
      on the pin of a commercial corona discharge needle by mean of a 1.3-cm long 
      stainless hollow tube. Odor sample driven by N(2) gas can be directly introduced 
      to the carbon fiber bundle to complete the ionization of analytes. Acetic acid, 
      ethyl acetate, ethyl caproate, octyl acetate, and damascone present in jujube 
      were selected to evaluate the performance of the CFI-MS method on quantitative 
      analysis of the gaseous sample. Good lineary was obtained (R(2) >/= 0.9946) between 
      5.0 and 500.0 ng/L with limits of detection (LOD) ranging from 0.5 to 1.5 ng/L. 
      Recoveries of five volatile compounds for the spiked jujube samples were between 
      94.36 and 106.74% with relative standard deviations (RSDs) less than 7.27% 
      (n = 5). Jujube of different varieties can be distinguished by principal 
      components analysis based on the analytical results of volatile compounds. The 
      developed method demonstrated obvious advantages such as simplicity, high 
      throughput, good sensitivity and wide range of applicability, which will be an 
      alternative way for in situ analysis of the odor sample.
CI  - (c) The Author(s) 2019.
FAU - Sun, Shihao
AU  - Sun S
AD  - 1Center for Chinese Medicine Therapy and Systems Biology, Shanghai University of 
      Traditional Chinese Medicine, Shanghai, 201203 China. ISNI: 0000 0001 2372 7462. 
      GRID: grid.412540.6
AD  - 2Key Laboratory in Flavor & Fragrance Basic Research, Zhengzhou Tobacco Research 
      Institute, China National Tobacco Corporation, Zhengzhou, 450001 China. ISNI: 
      0000 0004 0386 2036. GRID: grid.452261.6
FAU - Zhang, Yihan
AU  - Zhang Y
AD  - 2Key Laboratory in Flavor & Fragrance Basic Research, Zhengzhou Tobacco Research 
      Institute, China National Tobacco Corporation, Zhengzhou, 450001 China. ISNI: 
      0000 0004 0386 2036. GRID: grid.452261.6
FAU - Li, Peng
AU  - Li P
AD  - 2Key Laboratory in Flavor & Fragrance Basic Research, Zhengzhou Tobacco Research 
      Institute, China National Tobacco Corporation, Zhengzhou, 450001 China. ISNI: 
      0000 0004 0386 2036. GRID: grid.452261.6
FAU - Xi, Hui
AU  - Xi H
AD  - 2Key Laboratory in Flavor & Fragrance Basic Research, Zhengzhou Tobacco Research 
      Institute, China National Tobacco Corporation, Zhengzhou, 450001 China. ISNI: 
      0000 0004 0386 2036. GRID: grid.452261.6
FAU - Wu, Lei
AU  - Wu L
AD  - 2Key Laboratory in Flavor & Fragrance Basic Research, Zhengzhou Tobacco Research 
      Institute, China National Tobacco Corporation, Zhengzhou, 450001 China. ISNI: 
      0000 0004 0386 2036. GRID: grid.452261.6
FAU - Zhang, Jianxun
AU  - Zhang J
AD  - 2Key Laboratory in Flavor & Fragrance Basic Research, Zhengzhou Tobacco Research 
      Institute, China National Tobacco Corporation, Zhengzhou, 450001 China. ISNI: 
      0000 0004 0386 2036. GRID: grid.452261.6
FAU - Peng, Guixin
AU  - Peng G
AD  - Technology Center, China Tobacco Henan Industrial Co., Ltd., Zhengzhou, 450001 
      China.
FAU - Su, Yue
AU  - Su Y
AD  - 1Center for Chinese Medicine Therapy and Systems Biology, Shanghai University of 
      Traditional Chinese Medicine, Shanghai, 201203 China. ISNI: 0000 0001 2372 7462. 
      GRID: grid.412540.6
LA  - eng
PT  - Journal Article
DEP - 20191031
PL  - Switzerland
TA  - BMC Chem
JT  - BMC chemistry
JID - 101741142
PMC - PMC6823938
OTO - NOTNLM
OT  - Carbon fiber ionization mass spectrometry
OT  - In situ analysis
OT  - Jujube
OT  - Volatile
COIS- Competing interestsThe authors declare that they have no competing interests.
EDAT- 2019/11/07 06:00
MHDA- 2019/11/07 06:01
PMCR- 2019/10/31
CRDT- 2019/11/08 06:00
PHST- 2019/06/16 00:00 [received]
PHST- 2019/10/15 00:00 [accepted]
PHST- 2019/11/08 06:00 [entrez]
PHST- 2019/11/07 06:00 [pubmed]
PHST- 2019/11/07 06:01 [medline]
PHST- 2019/10/31 00:00 [pmc-release]
AID - 641 [pii]
AID - 10.1186/s13065-019-0641-4 [doi]
PST - epublish
SO  - BMC Chem. 2019 Oct 31;13(1):125. doi: 10.1186/s13065-019-0641-4. eCollection 2019 
      Dec.