PMID- 31904006
OWN - NLM
STAT- MEDLINE
DCOM- 20201207
LR  - 20230808
IS  - 1348-2246 (Electronic)
IS  - 0910-6340 (Linking)
VI  - 36
IP  - 4
DP  - 2020 Apr 10
TI  - Rapid Determination of 17 Phthalate Esters in Capsanthin by QuEChERS Coupled with 
      Gas Chromatography-Mass Spectrometry.
PG  - 485-490
LID - 10.2116/analsci.19P421 [doi]
AB  - A method for the simultaneous determination of 17 kinds of phthalate esters in 
      capsanthin was developed by the QuEChERS (quick, easy, cheap, effective, 
      ruggedand safe) pretreatment method coupled with gas chromatography-mass 
      spectrometry(GC-MS). Capsanthin samples were extracted with acetonitrile, and 
      then sodium chloride and anhydrous magnesium sulfate were added for salting out. 
      After the extracting liquids were cleansed by florisil, the supernatants were 
      analyzed by GC-MS. The limits of detection (LOD) and limits of quantitation (LOQ) 
      ranged from 0.2 to 0.5 mug/g and 0.6 to 1.5 mug/g, respectively. DMP, DEP, DAP, 
      DIBP, DBP, BMPP, DPP, DHXP and DCHP were in the range of 0.2 - 10 mug/g; DMEP, 
      DEEP, BBP, DBEP, DEHP, DPhP, DNOP and DNP were in the range of 0.5 - 20 mug/g. And 
      all had good linearity and the linear correlation coefficients (R(2)) were more 
      than 0.995. The average recoveries of 17 kinds of PAEs of the three levels were 
      between 82.8 and 118.1%, and the relative standard deviations (RSDs) were between 
      0.12 and 7.3%. It is a simple, rapid, accurate and reliable method for the rapid 
      detection of PAEs in large quantities of natural plant extract samples.
FAU - Niu, Yuqi
AU  - Niu Y
AD  - College of Biological Science and Engineering, Hebei University of Science and 
      Technology, Shijiazhuang, 050018, China.
FAU - Gao, Wenhui
AU  - Gao W
AD  - College of Biological Science and Engineering, Hebei University of Science and 
      Technology, Shijiazhuang, 050018, China. wenhuigao@126.com.
FAU - Li, Hui
AU  - Li H
AD  - Hebei Insitute of Medical Equipment and Drugs Packaging Material Inspection, 
      Shijiazhuang, 050061, China. lihui7171@163.com.
FAU - Zhang, Jingxuan
AU  - Zhang J
AD  - Hebei Guanzhuo Testing Technology Co., Ltd, Shijiazhuang, 051130, China.
FAU - Lian, Yunhe
AU  - Lian Y
AD  - Chenguang Biotechnology Group Co., Ltd, Shijiazhuang, 057250, China.
LA  - eng
PT  - Journal Article
DEP - 20200103
PL  - Switzerland
TA  - Anal Sci
JT  - Analytical sciences : the international journal of the Japan Society for 
      Analytical Chemistry
JID - 8511078
RN  - 0 (Esters)
RN  - 0 (Phthalic Acids)
RN  - 0 (Xanthophylls)
RN  - 420NY1J57N (capsanthin)
RN  - 6O7F7IX66E (phthalic acid)
SB  - IM
MH  - Esters/*analysis
MH  - Gas Chromatography-Mass Spectrometry
MH  - Phthalic Acids/*analysis
MH  - Xanthophylls/chemistry
OTO - NOTNLM
OT  - Capsanthin
OT  - QuEChERS
OT  - gas chromatography-mass spectrometry
OT  - phthalate esters
OT  - rapid detection
EDAT- 2020/01/07 06:00
MHDA- 2020/12/15 06:00
CRDT- 2020/01/07 06:00
PHST- 2020/01/07 06:00 [pubmed]
PHST- 2020/12/15 06:00 [medline]
PHST- 2020/01/07 06:00 [entrez]
AID - 10.2116/analsci.19P421 [pii]
AID - 10.2116/analsci.19P421 [doi]
PST - ppublish
SO  - Anal Sci. 2020 Apr 10;36(4):485-490. doi: 10.2116/analsci.19P421. Epub 2020 Jan 
      3.