PMID- 31935982 OWN - NLM STAT- PubMed-not-MEDLINE LR - 20201001 IS - 1996-1944 (Print) IS - 1996-1944 (Electronic) IS - 1996-1944 (Linking) VI - 13 IP - 1 DP - 2020 Jan 6 TI - Preparation and Characterization of Alumina HDPE Composites. LID - 10.3390/ma13010250 [doi] LID - 250 AB - In this study, effects of two different types of porous alumina nanoparticles have been incorporated into high-density polyethylene (HDPE) to study their impact on the properties of the HDPE composite. The dispersion of fillers in the HDPE matrix was evaluated by scanning electron microscopy (SEM). Differential scanning calorimetry (DSC) and thermogravimetric analyzer (TGA) integrated with Fourier transform infrared spectroscopy (FTIR) were applied to investigate the calorimetric behavior and thermal stability and to analyze the polymer decomposition, respectively. The dielectric properties were determined by a broadband dielectric spectroscopy. The effect of filler loading on the tensile properties and melt flow index was also examined. A homogenous distribution of the fillers was observed at low loading of alumina particles (below 5 wt. %). However, agglomerates of sub-micro size were formed extensively on samples with high loading of fillers (above 7 wt. %). A significant improvement of the thermo-oxidation stability of the composite was observed. The permittivity values of the prepared composites also increased with the addition of the fillers. The incorporation of fillers also increased the electrical conductivity values of the prepared composites at high frequencies. FAU - Saleh, Mohamed AU - Saleh M AD - Centre for Advanced Materials, Qatar University, Doha 2713, Qatar. FAU - Al-Hajri, Zainab AU - Al-Hajri Z AD - Department of Chemistry and Earth Science, Qatar University, Doha 2713, Qatar. FAU - Popelka, Anton AU - Popelka A AD - Centre for Advanced Materials, Qatar University, Doha 2713, Qatar. FAU - Javaid Zaidi, Syed AU - Javaid Zaidi S AD - Centre for Advanced Materials, Qatar University, Doha 2713, Qatar. LA - eng PT - Journal Article DEP - 20200106 PL - Switzerland TA - Materials (Basel) JT - Materials (Basel, Switzerland) JID - 101555929 PMC - PMC6981892 OTO - NOTNLM OT - high-density polyethylene (HDPE) OT - morphology OT - porous alumina nanoparticles OT - thermal properties COIS- The authors declare no conflict of interest. EDAT- 2020/01/16 06:00 MHDA- 2020/01/16 06:01 PMCR- 2020/01/06 CRDT- 2020/01/16 06:00 PHST- 2019/11/18 00:00 [received] PHST- 2019/12/22 00:00 [revised] PHST- 2020/01/02 00:00 [accepted] PHST- 2020/01/16 06:00 [entrez] PHST- 2020/01/16 06:00 [pubmed] PHST- 2020/01/16 06:01 [medline] PHST- 2020/01/06 00:00 [pmc-release] AID - ma13010250 [pii] AID - materials-13-00250 [pii] AID - 10.3390/ma13010250 [doi] PST - epublish SO - Materials (Basel). 2020 Jan 6;13(1):250. doi: 10.3390/ma13010250.