PMID- 32099973
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20220413
IS  - 2661-801X (Electronic)
IS  - 2661-801X (Linking)
VI  - 14
IP  - 1
DP  - 2020 Dec
TI  - A simple strategy based on fibers coated with surfactant-functionalized 
      multiwalled carbon nanotubes to improve the properties of solid-phase 
      microextraction of phenols in aqueous solution.
PG  - 15
LID - 10.1186/s13065-020-00665-7 [doi]
LID - 15
AB  - METHODS AND EXPERIMENTS: In this study, a functionalized multiwalled carbon 
      nanotube (MWCNT)-coated solid-phase microextraction (SPME) fiber was developed 
      for concentrating analytes in aqueous samples. Sodium deoxycholate (NaDC) was 
      used as a dispersing agent for non-covalent modification of MWCNTs. The coating 
      showed porous structure and large adsorption capacity. To investigate the 
      capability of this MWCNTs/NaDC SPME fiber, it was applied to the analysis of 
      phenols in aqueous solution. After extraction, the analytes were desorbed in an 
      acetonitrile-water solution and analyzed using high-performance liquid 
      chromatography. RESULTS: The MWCNTs/NaDC fiber exhibited good analytical 
      performance, and fine preparation reproducibility was obtained with the relative 
      standard deviations (RSDs) ranging from 4.9% to 10.2% (n = 6) in one batch, from 
      5.7% to 11.9% (n = 3) among different batches. Under the optimum extraction 
      conditions, the detection limits were 0.15-0.30 ng/mL(S/N = 3), the linear 
      detection ranges were 1-100 ng/mL (R(2) >/= 0.9997) for these analytes, and good 
      recoveries (80.3-95.4%) were obtained for the spiked samples. CONCLUSION: This is 
      a simple and accurate pretreatment method for the analysis of phenols in aqueous 
      samples.
CI  - (c) The Author(s) 2020.
FAU - Zhou, Xueqing
AU  - Zhou X
AUID- ORCID: 0000-0001-7654-6286
AD  - 1Analytical and Testing Center, Hainan University, Haikou, 570228 China. GRID: 
      grid.428986.9. ISNI: 0000 0001 0373 6302
AD  - 2College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 
      China. GRID: grid.428986.9. ISNI: 0000 0001 0373 6302
FAU - Xie, Yanli
AU  - Xie Y
AD  - 1Analytical and Testing Center, Hainan University, Haikou, 570228 China. GRID: 
      grid.428986.9. ISNI: 0000 0001 0373 6302
FAU - Zhao, Zhendong
AU  - Zhao Z
AD  - 1Analytical and Testing Center, Hainan University, Haikou, 570228 China. GRID: 
      grid.428986.9. ISNI: 0000 0001 0373 6302
FAU - Fu, Wenyan
AU  - Fu W
AD  - 2College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 
      China. GRID: grid.428986.9. ISNI: 0000 0001 0373 6302
LA  - eng
PT  - Journal Article
DEP - 20200219
PL  - Switzerland
TA  - BMC Chem
JT  - BMC chemistry
JID - 101741142
PMC - PMC7029595
OTO - NOTNLM
OT  - Functionalized multiwalled carbon nanotube
OT  - Phenol
OT  - Solid-phase microextraction
OT  - Surfactant
COIS- Competing interestsThe authors declare that they have no competing interest.
EDAT- 2020/02/27 06:00
MHDA- 2020/02/27 06:01
PMCR- 2020/02/19
CRDT- 2020/02/27 06:00
PHST- 2019/07/14 00:00 [received]
PHST- 2020/01/30 00:00 [accepted]
PHST- 2020/02/27 06:00 [entrez]
PHST- 2020/02/27 06:00 [pubmed]
PHST- 2020/02/27 06:01 [medline]
PHST- 2020/02/19 00:00 [pmc-release]
AID - 665 [pii]
AID - 10.1186/s13065-020-00665-7 [doi]
PST - epublish
SO  - BMC Chem. 2020 Feb 19;14(1):15. doi: 10.1186/s13065-020-00665-7. eCollection 2020 
      Dec.