PMID- 32138247
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20240328
IS  - 1996-1944 (Print)
IS  - 1996-1944 (Electronic)
IS  - 1996-1944 (Linking)
VI  - 13
IP  - 5
DP  - 2020 Mar 3
TI  - Facile Synthesis of Super-Microporous Titania-Alumina with Tailored Framework 
      Properties.
LID - 10.3390/ma13051126 [doi]
LID - 1126
AB  - Super-microporous material (pore size 1-2 nm) can bridge the pore size gap 
      between the zeolites (<1 nm) and the mesoporous oxides (>2 nm). A series of 
      super-microporous titania-alumina materials has been successfully prepared via a 
      facile one-pot evaporation-induced self-assembly (EISA) strategy by different 
      solvents using fatty alcohol polyoxyethylene ether (AEO-7) as the template. 
      Moreover, no extra acid or base is added in our synthesis process. When titanium 
      isopropylate is used as the titanium source, these materials exhibit high BET 
      surface areas (from 275 to 396 m(2)/g) and pore volumes (from 0.14 to 0.18 
      cm(3)/g). The sample prepared using methanol as the solvent shows the largest 
      Brunauer-Emmett-Teller (BET) surface area of 396 m(2)/g. When tetrabutyl titanate 
      is used as the titanium source, these materials exhibit high BET surface areas 
      (from 282 to 396 m(2)/g) and pore volumes (from 0.13 to 0.18 cm(3)/g). The sample 
      prepared using ethanol as the solvent shows the largest BET surface area of 396 
      m(2)/g.
FAU - Li, Yongfeng
AU  - Li Y
AD  - New Energy Engineering, Shanxi Institute of Energy, Jinzhong 030600, China.
AD  - College of Chemistry and Chemical Engineering, Taiyuan University of Technology, 
      Taiyuan 030024, China.
FAU - Su, Jiaojiao
AU  - Su J
AD  - College of Chemistry and Chemical Engineering, Taiyuan University of Technology, 
      Taiyuan 030024, China.
FAU - Li, Guiping
AU  - Li G
AD  - New Energy Engineering, Shanxi Institute of Energy, Jinzhong 030600, China.
FAU - Meng, Xiufeng
AU  - Meng X
AD  - New Energy Engineering, Shanxi Institute of Energy, Jinzhong 030600, China.
LA  - eng
GR  - ZB-2018004/The School Fund/
PT  - Journal Article
DEP - 20200303
PL  - Switzerland
TA  - Materials (Basel)
JT  - Materials (Basel, Switzerland)
JID - 101555929
PMC - PMC7085005
OTO - NOTNLM
OT  - different solvents
OT  - fatty alcohol polyoxyethylene ether
OT  - high BET surface areas
OT  - super-microporous alumina-titania
COIS- The authors declare no conflict of interest.
EDAT- 2020/03/07 06:00
MHDA- 2020/03/07 06:01
PMCR- 2020/03/03
CRDT- 2020/03/07 06:00
PHST- 2020/01/20 00:00 [received]
PHST- 2020/02/20 00:00 [revised]
PHST- 2020/02/25 00:00 [accepted]
PHST- 2020/03/07 06:00 [entrez]
PHST- 2020/03/07 06:00 [pubmed]
PHST- 2020/03/07 06:01 [medline]
PHST- 2020/03/03 00:00 [pmc-release]
AID - ma13051126 [pii]
AID - materials-13-01126 [pii]
AID - 10.3390/ma13051126 [doi]
PST - epublish
SO  - Materials (Basel). 2020 Mar 3;13(5):1126. doi: 10.3390/ma13051126.