PMID- 33326928 OWN - NLM STAT- MEDLINE DCOM- 20210126 LR - 20210126 IS - 1873-3778 (Electronic) IS - 0021-9673 (Linking) VI - 1636 DP - 2021 Jan 11 TI - Ultrasound-assisted dispersive solid-phase extraction combined with reversed-phase high-performance liquid chromatography-photodiode array detection for the determination of nine biogenic amines in canned seafood. PG - 461768 LID - S0021-9673(20)31042-6 [pii] LID - 10.1016/j.chroma.2020.461768 [doi] AB - This work describes an ultrasound-assisted dispersive solid-phase extraction method combined with reversed-phase high-performance liquid chromatography-photodiode array detection (UADSPE-RPLC-PDA) for the determination of nine common biogenic amines (BAs) in canned seafood. The pretreatment extraction solvent, ultrasonic treatment duration, and derivatization conditions were optimized. The method was validated on the basis of the limit of detection (LOD), limit of quantification (LOQ), precision, and accuracy and successfully applied to analyze four canned fish, two canned shrimp and four canned shellfish samples. LODs of 0.08-0.25 mg kg(-1) were achieved, and the correlation coefficient of determination was 0.9994-0.9997. The method had high precision and accuracy, with relative standard deviations (RSDs) and recoveries of 0.44 to 6.83% and 72.57 to 99.74%, respectively, suggesting the effectiveness of ultrasound-assisted extraction at increasing the solubility of the target analytes in the solvent system and the feasibility of UADSPE-RPLC-PDA for determining trace BAs in canned seafood. CI - Copyright (c) 2020 Elsevier B.V. All rights reserved. FAU - Wang, Jingyu AU - Wang J AD - Shanghai Engineering Research Center of Aquatic Product Processing and Preservation, College of Food Science and Technology, Shanghai Ocean University, Shanghai 200120, China. FAU - Liu, Zhidong AU - Liu Z AD - Key Laboratory of Oceanic and Polar Fisheries, Ministry of Agriculture and Rural Affair, East China Sea Fishery Research Institute, Chinese Academy of Fishery Sciences, Shanghai 200090, China. Electronic address: zd-liu@hotmail.com. FAU - Qu, Yinghong AU - Qu Y AD - Shanghai Engineering Research Center of Aquatic Product Processing and Preservation, College of Food Science and Technology, Shanghai Ocean University, Shanghai 200120, China. Electronic address: yhqu@shou.edu.cn. LA - eng PT - Journal Article DEP - 20201130 PL - Netherlands TA - J Chromatogr A JT - Journal of chromatography. A JID - 9318488 RN - 0 (Biogenic Amines) RN - 0 (Solvents) SB - IM MH - Animals MH - Biogenic Amines/*analysis/isolation & purification MH - Chromatography, High Pressure Liquid/*methods MH - Chromatography, Reverse-Phase MH - Limit of Detection MH - Seafood/*analysis MH - Solid Phase Extraction MH - Solvents/chemistry MH - Sonication OTO - NOTNLM OT - Biogenic amines OT - Canned seafood OT - HPLC OT - Ultrasound-assisted dispersive solid-phase extraction COIS- Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper. EDAT- 2020/12/17 06:00 MHDA- 2021/01/27 06:00 CRDT- 2020/12/16 20:08 PHST- 2020/08/22 00:00 [received] PHST- 2020/11/24 00:00 [revised] PHST- 2020/11/25 00:00 [accepted] PHST- 2020/12/17 06:00 [pubmed] PHST- 2021/01/27 06:00 [medline] PHST- 2020/12/16 20:08 [entrez] AID - S0021-9673(20)31042-6 [pii] AID - 10.1016/j.chroma.2020.461768 [doi] PST - ppublish SO - J Chromatogr A. 2021 Jan 11;1636:461768. doi: 10.1016/j.chroma.2020.461768. Epub 2020 Nov 30.