PMID- 34049048
OWN - NLM
STAT- MEDLINE
DCOM- 20210706
LR  - 20210706
IS  - 1873-7072 (Electronic)
IS  - 0308-8146 (Linking)
VI  - 361
DP  - 2021 Nov 1
TI  - Determination of 8 biogenic amines in aquatic products and their derived products 
      by high-performance liquid chromatography-tandem mass spectrometry without 
      derivatization.
PG  - 130044
LID - S0308-8146(21)01050-5 [pii]
LID - 10.1016/j.foodchem.2021.130044 [doi]
AB  - A method for the determination of 8 biogenic amines in aquatic products and their 
      derived products was established by HPLC-MS/MS without derivatization. The 
      samples were extracted by 5% perchloric acid solution. N-hexane was used to clean 
      the extract. The analytes were separated by a column of ACQUITY UPLC HSS T3 
      (100 mm x 2.1 mm, 1.8 microm), and gradient eluted with a mixed solution of (0.5% 
      formic acid) and acetonitrile. Good linearity was obtained with correlation 
      coefficients (R(2)) >0.99. This method achieved higher sensitivity (from 
      0.1 mg/kg for tyramine, 2-phenylethylamine and tryptamine to 1.0 mg/kg for 
      spermidine, spermine, cadaverin, histamine and putrescine). The average 
      recoveries were demonstrated in the range of 70.9%-113.1%, with relative standard 
      deviations (RSDs) from 0.33% to 10.81%. This method was suitable for the 
      detection of BAs in aquatic products and their products.
CI  - Copyright (c) 2021 Elsevier Ltd. All rights reserved.
FAU - Zhang, Xuan
AU  - Zhang X
AD  - Key Laboratory of East China Sea Fishery Resources Exploitation, Ministry of 
      Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, 
      Chinese Academy of Fishery Sciences, Shanghai 200090, China.
FAU - Fang, Changling
AU  - Fang C
AD  - Key Laboratory of East China Sea Fishery Resources Exploitation, Ministry of 
      Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, 
      Chinese Academy of Fishery Sciences, Shanghai 200090, China.
FAU - Huang, Dongmei
AU  - Huang D
AD  - Key Laboratory of East China Sea Fishery Resources Exploitation, Ministry of 
      Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, 
      Chinese Academy of Fishery Sciences, Shanghai 200090, China.
FAU - Yang, Guangxin
AU  - Yang G
AD  - Key Laboratory of East China Sea Fishery Resources Exploitation, Ministry of 
      Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, 
      Chinese Academy of Fishery Sciences, Shanghai 200090, China.
FAU - Tang, Yunyu
AU  - Tang Y
AD  - Key Laboratory of East China Sea Fishery Resources Exploitation, Ministry of 
      Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, 
      Chinese Academy of Fishery Sciences, Shanghai 200090, China.
FAU - Shi, Yongfu
AU  - Shi Y
AD  - Key Laboratory of East China Sea Fishery Resources Exploitation, Ministry of 
      Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, 
      Chinese Academy of Fishery Sciences, Shanghai 200090, China.
FAU - Kong, Cong
AU  - Kong C
AD  - Key Laboratory of East China Sea Fishery Resources Exploitation, Ministry of 
      Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, 
      Chinese Academy of Fishery Sciences, Shanghai 200090, China.
FAU - Cao, Pei
AU  - Cao P
AD  - NHC Key Laboratory of Food Safety Risk Assessment, Food Safety Research Unit 
      (2019RU014) of Chinese Academy of Medical Science, China National Center for Food 
      Safety Risk Assessment, Beijing 100021, China. Electronic address: 
      apple_caopei@126.com.
FAU - Cai, Youqiong
AU  - Cai Y
AD  - Key Laboratory of East China Sea Fishery Resources Exploitation, Ministry of 
      Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, 
      Chinese Academy of Fishery Sciences, Shanghai 200090, China. Electronic address: 
      caiyouqiong@163.com.
LA  - eng
PT  - Journal Article
DEP - 20210511
PL  - England
TA  - Food Chem
JT  - Food chemistry
JID - 7702639
RN  - 0 (Biogenic Amines)
RN  - 0 (Phenethylamines)
RN  - 0 (Tryptamines)
RN  - 2FZ7Y3VOQX (Spermine)
RN  - 327C7L2BXQ (phenethylamine)
RN  - 422ZU9N5TV (tryptamine)
RN  - 820484N8I3 (Histamine)
RN  - L90BEN6OLL (Cadaverine)
RN  - U87FK77H25 (Spermidine)
RN  - V10TVZ52E4 (Putrescine)
RN  - X8ZC7V0OX3 (Tyramine)
SB  - IM
MH  - Biogenic Amines/*analysis
MH  - Cadaverine/analysis
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Histamine/analysis
MH  - Phenethylamines/analysis
MH  - Putrescine/analysis
MH  - Seafood/*analysis
MH  - Spermidine/analysis
MH  - Spermine/analysis
MH  - Tandem Mass Spectrometry/*methods
MH  - Tryptamines/analysis
MH  - Tyramine/analysis
OTO - NOTNLM
OT  - Aquatic products
OT  - Biogenic amines
OT  - High-performance liquid chromatography-tandem mass spectrometry
EDAT- 2021/05/29 06:00
MHDA- 2021/07/07 06:00
CRDT- 2021/05/28 20:18
PHST- 2021/02/09 00:00 [received]
PHST- 2021/04/09 00:00 [revised]
PHST- 2021/05/05 00:00 [accepted]
PHST- 2021/05/29 06:00 [pubmed]
PHST- 2021/07/07 06:00 [medline]
PHST- 2021/05/28 20:18 [entrez]
AID - S0308-8146(21)01050-5 [pii]
AID - 10.1016/j.foodchem.2021.130044 [doi]
PST - ppublish
SO  - Food Chem. 2021 Nov 1;361:130044. doi: 10.1016/j.foodchem.2021.130044. Epub 2021 
      May 11.