PMID- 34213140
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20210702
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 37
IP  - 12
DP  - 2019 Dec 8
TI  - [Determination of diethyl aminoethyl hexanoate residues in apples by gas 
      chromatography-mass spectrometry combined with improved QuEChERS].
PG  - 1363-1367
LID - 10.3724/SP.J.1123.2019.08021 [doi]
AB  - A method was developed for the determination of diethyl aminoethyl hexanoate 
      (DA-6) residues in apples by gas chromatography-mass spectrometry (GC-MS) 
      combined with improved QuEChERS. The samples were first extracted with warm 
      water, then, the extract was subjected to liquid-liquid re-extraction with 
      dichloromethane, followed by rotary evaporation concentration. The residues were 
      cleaned up with primary secondary amine (PSA). The analytes were separated on an 
      HP-5 capillary column and detected using an EI source in the SIM mode. The 
      recoveries ranged from 74.1% to 84.2% at three spiked levels, with relative 
      standard deviations (RSDs) between 1.5% and 4.1%. The limit of detection and 
      limit of quantification were 0.0024 mg/kg and 0.008 mg/kg, respectively. The 
      developed method is sensitive, and practically applicable for the determination 
      of DA-6 residues in apple samples.
FAU - Kong, Xiangji
AU  - Kong X
AD  - Nanjing Institute of Environmental Science, Ministry of Ecology and Environment 
      of the People's Republic of China, Nanjing 210042, China.
FAU - Kong, Shun
AU  - Kong S
AD  - School of Civil Engineering, Southeast University, Nanjing 211189, China.
FAU - Zhang, Xuemei
AU  - Zhang X
AD  - Jiangsu Institute of Metrology, Nanjing 210023, China.
FAU - Kong, Deyang
AU  - Kong D
AD  - Nanjing Institute of Environmental Science, Ministry of Ecology and Environment 
      of the People's Republic of China, Nanjing 210042, China.
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
SB  - IM
OTO - NOTNLM
OT  - QuEChERS
OT  - apple
OT  - diethyl aminoethyl hexanoate (DA-6)
OT  - gas chromatography-mass spectrometry (GC-MS)
EDAT- 2019/12/08 00:00
MHDA- 2019/12/08 00:01
CRDT- 2021/07/02 09:12
PHST- 2021/07/02 09:12 [entrez]
PHST- 2019/12/08 00:00 [pubmed]
PHST- 2019/12/08 00:01 [medline]
AID - 10.3724/SP.J.1123.2019.08021 [doi]
PST - ppublish
SO  - Se Pu. 2019 Dec 8;37(12):1363-1367. doi: 10.3724/SP.J.1123.2019.08021.