PMID- 34213143
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20210702
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 37
IP  - 12
DP  - 2019 Dec 8
TI  - [Rapid analysis of the specific migration of seven terephthalates and benzoates 
      from plastic food contact material and products by high performance liquid 
      chromatography-ultraviolet detection].
PG  - 1383-1391
LID - 10.3724/SP.J.1123.2019.06021 [doi]
AB  - A method based on high-performance liquid chromatography-ultraviolet (HPLC-UV) 
      detection was developed for the rapid analysis of the specific migration of seven 
      terephthalates and benzoates (TPBAs) in seven food simulants (10% (v/v) ethanol, 
      3% (m/v, i. e. 3 g/100 mL) acetic acid, 4% (v/v) acetic acid, 20% (v/v) ethanol, 
      50% (v/v) ethanol, 95% (v/v) ethanol, or olive oil)). Detailed comparisons were 
      made on the extraction or purification of the seven TPBAs in olive oil food 
      simulants by solvents, QuEChERS dSPE EMR-Lipid technology, and Captiva EMR-Lipid 
      technology. The seven TPBAs were separated completely within 17 min by gradient 
      elution on a phenyl column using water and methanol as the mobile phase. The 
      detection wavelength was set at 237 nm. The injection volume was 10 muL. The 
      linearities of the seven TPBAs were good, with r>/=0.9998 at 1-80 mg/L or 8-160 
      mg/kg in the seven food simulants. The average recoveries of the seven TPBAs were 
      between 91.7% and 106%, with relative standard deviations (RSDs) between 0.1% and 
      3.1% (n=6). The limits of quantification were 0.2-8.1 mg/kg. This method is 
      simple, with convenient pretreatments, good chromatographic separation and linear 
      relationships, as well as satisfactory recoveries and RSDs. The method has been 
      applied to detect the specific migration of the seven TPBAs in real samples.
FAU - Xiao, Xiaofeng
AU  - Xiao X
AD  - Taizhou Customs Comprehensive Technology Service Center, Taizhou 318000, China.
FAU - Wang, Jianling
AU  - Wang J
AD  - Taizhou Customs Comprehensive Technology Service Center, Taizhou 318000, China.
FAU - Liu, Tingfei
AU  - Liu T
AD  - Taizhou Customs Comprehensive Technology Service Center, Taizhou 318000, China.
FAU - He, Jun
AU  - He J
AD  - Taizhou Customs Comprehensive Technology Service Center, Taizhou 318000, China.
FAU - Chen, Tong
AU  - Chen T
AD  - Taizhou Customs Comprehensive Technology Service Center, Taizhou 318000, China.
FAU - Wang, Ji
AU  - Wang J
AD  - Taizhou Customs Comprehensive Technology Service Center, Taizhou 318000, China.
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
SB  - IM
OTO - NOTNLM
OT  - benzoate
OT  - high performance liquid chromatography-ultraviolet detection (HPLC-UV)
OT  - specific migration
OT  - terephthalate
EDAT- 2019/12/08 00:00
MHDA- 2019/12/08 00:01
CRDT- 2021/07/02 09:12
PHST- 2021/07/02 09:12 [entrez]
PHST- 2019/12/08 00:00 [pubmed]
PHST- 2019/12/08 00:01 [medline]
AID - 10.3724/SP.J.1123.2019.06021 [doi]
PST - ppublish
SO  - Se Pu. 2019 Dec 8;37(12):1383-1391. doi: 10.3724/SP.J.1123.2019.06021.