PMID- 34213216
OWN - NLM
STAT- MEDLINE
DCOM- 20210716
LR  - 20210716
IS  - 1872-2059 (Electronic)
IS  - 1000-8713 (Linking)
VI  - 38
IP  - 3
DP  - 2020 Mar 8
TI  - [Simultaneous determination of inorganic anions and cations in wine by capillary 
      electrophoresis-indirect ultraviolet detection with ionic liquid as background 
      electrolyte].
PG  - 356-361
LID - 10.3724/SP.J.1123.2019.09010 [doi]
AB  - A novel method was developed for the simultaneous determination of inorganic 
      anions (Cl(-), SO(4)(2-) and ClO(3)(-)) and cations (K(+), Ca(2+), Na(+), Mg(2+) 
      and Li(+)) in wine by capillary electrophoresis-indirect ultraviolet detection 
      (CE-UV) with dual-opposite end injection using 1-ethyl-3-methylimidazolium 
      p-toluenesulfonate ([EMIm]TS) as the background electrolyte.[EMIm]TS acted as the 
      running electrolyte and probe, generating the background signals for cations and 
      anions under indirect UV light, consequently simplifying the electrophoretic 
      medium. Under the optimal experimental conditions, baseline separation was 
      achieved for the eight inorganic ions within 6.5 min. The linear ranges of the 
      eight inorganic ions were 0.005-0.7 g/L, with correlation coefficients (R(2)) of 
      0.963-0.995. The limits of detection (LODs) were between 1.2 and 12.5 mg/L at a 
      signal-to-noise ratio of 3 (S/N=3). Eight inorganic ions were detected in three 
      different brands of wines obtained from supermarket. Good recoveries of 
      90.1%-110.5% at three spiked levels (0.05, 0.2 and 0.4 g/L) were achieved with a 
      low relative standard deviations (RSDs) (n=5) of 1.1%-4.8%. The proposed method 
      is robust and reliable for the sensitive and rapid analysis of the inorganic 
      anions and cations, and it has potential in evaluating the quality of wine.
FAU - Tian, Miaomiao
AU  - Tian M
AD  - Institute of Chemical and Industrial Bioengineering, Jilin Engineering Normal 
      University, Changchun, 130052, China.
FAU - Liu, Xin
AU  - Liu X
AD  - Faculty of Chemistry, Northeast Normal University, Changchun, 130024, China.
FAU - Yang, Li
AU  - Yang L
AD  - Faculty of Chemistry, Northeast Normal University, Changchun, 130024, China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Anions)
RN  - 0 (Cations)
RN  - 0 (Electrolytes)
RN  - 0 (Ionic Liquids)
SB  - IM
MH  - *Anions/analysis
MH  - *Cations/analysis
MH  - Electrolytes
MH  - Electrophoresis, Capillary
MH  - *Food Analysis
MH  - Ionic Liquids
MH  - Ultraviolet Rays
MH  - *Wine/analysis
OTO - NOTNLM
OT  - anions
OT  - capillary electrophoresis (CE)
OT  - cations
OT  - indirect ultraviolet detection
OT  - ionic liquids
OT  - wine
EDAT- 2020/03/08 00:00
MHDA- 2021/07/17 06:00
CRDT- 2021/07/02 09:12
PHST- 2021/07/02 09:12 [entrez]
PHST- 2020/03/08 00:00 [pubmed]
PHST- 2021/07/17 06:00 [medline]
AID - 10.3724/SP.J.1123.2019.09010 [doi]
PST - ppublish
SO  - Se Pu. 2020 Mar 8;38(3):356-361. doi: 10.3724/SP.J.1123.2019.09010.