PMID- 34359521
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20240402
IS  - 2304-8158 (Print)
IS  - 2304-8158 (Electronic)
IS  - 2304-8158 (Linking)
VI  - 10
IP  - 7
DP  - 2021 Jul 16
TI  - Rapid Screening of 350 Pesticide Residues in Vegetable and Fruit Juices by 
      Multi-Plug Filtration Cleanup Method Combined with Gas 
      Chromatography-Electrostatic Field Orbitrap High Resolution Mass Spectrometry.
LID - 10.3390/foods10071651 [doi]
LID - 1651
AB  - A new method for screening pesticide residues in vegetable and fruit juices by 
      the multi-plug filtration cleanup (m-PFC) method combined with gas 
      chromatography-electrostatic field orbitrap high resolution mass 
      spectrometry(GC-Orbitrap/MS) was developed. The samples were extracted with 
      acetonitrile, purified with m-PFC and determined by GC-Orbitrap/MS. Qualitative 
      analysis was confirmed by retention time, accurate molecular mass and 
      quantitative analysis were performed with the matrix standard calibration. It 
      could eliminate matrix interference effectively. Eight kinds of typical samples 
      (orange juice, apple juice, grape juice, strawberry juice, celery juice, carrot 
      juice, cucumber juice, tomato juice) were evaluated. The linear ranges of the 350 
      pesticides were from 5 to 500 mug/kg, with good correlation coefficients greater 
      than 0.990. The limits of detection (LODs) were 0.3-3.0 mug/kg and the limits of 
      quantification (LOQs) were 1.0-10.0 mug/kg. The average recoveries at three spiked 
      levels of 10, 100, 200 mug/kg were in the range of 72.8-122.4%, with relative 
      standard deviations (RSDs) of 2.0-10.8%. The method has effectively improved the 
      determination efficiency of pesticide residue screening by high-resolution mass 
      spectrometry in vegetable and fruit juices.
FAU - Meng, Zhijuan
AU  - Meng Z
AD  - Key Laboratory of Food Safety of Hebei Province, Hebei Food Inspection and 
      Research Institute, Shijiazhuang 050091, China.
FAU - Li, Qiang
AU  - Li Q
AD  - Key Laboratory of Food Safety of Hebei Province, Hebei Food Inspection and 
      Research Institute, Shijiazhuang 050091, China.
FAU - Cong, Jianhan
AU  - Cong J
AD  - Beijing Key Laboratory of Environmental and Viral Oncology, Faculty of 
      Environment and Life, Beijing University of Technology, Beijing 100124, China.
FAU - Huang, Yunxia
AU  - Huang Y
AD  - Key Laboratory of Food Safety of Hebei Province, Hebei Food Inspection and 
      Research Institute, Shijiazhuang 050091, China.
FAU - Wang, Dong
AU  - Wang D
AD  - Key Laboratory of Food Safety of Hebei Province, Hebei Food Inspection and 
      Research Institute, Shijiazhuang 050091, China.
FAU - Pan, Canping
AU  - Pan C
AD  - Department of Applied Chemistry, College of Science, China Agricultural 
      University, Beijing 100193, China.
FAU - Fan, Sufang
AU  - Fan S
AD  - Key Laboratory of Food Safety of Hebei Province, Hebei Food Inspection and 
      Research Institute, Shijiazhuang 050091, China.
FAU - Zhang, Yan
AU  - Zhang Y
AUID- ORCID: 0000-0002-2947-1629
AD  - Key Laboratory of Food Safety of Hebei Province, Hebei Food Inspection and 
      Research Institute, Shijiazhuang 050091, China.
LA  - eng
GR  - 2018YFC1603400/National Key Research and Development Program of China/
GR  - 2019YJ009/State Administration for Market Regulation Special Technical Support 
      Program/
PT  - Journal Article
DEP - 20210716
PL  - Switzerland
TA  - Foods
JT  - Foods (Basel, Switzerland)
JID - 101670569
PMC - PMC8305287
OTO - NOTNLM
OT  - GC-Orbitrap/MS
OT  - m-PFC
OT  - pesticide residues
OT  - rapid screening
OT  - vegetable and fruit juices
COIS- The authors declare no conflict of interest.
EDAT- 2021/08/08 06:00
MHDA- 2021/08/08 06:01
PMCR- 2021/07/16
CRDT- 2021/08/07 01:03
PHST- 2021/05/08 00:00 [received]
PHST- 2021/06/20 00:00 [revised]
PHST- 2021/07/06 00:00 [accepted]
PHST- 2021/08/07 01:03 [entrez]
PHST- 2021/08/08 06:00 [pubmed]
PHST- 2021/08/08 06:01 [medline]
PHST- 2021/07/16 00:00 [pmc-release]
AID - foods10071651 [pii]
AID - foods-10-01651 [pii]
AID - 10.3390/foods10071651 [doi]
PST - epublish
SO  - Foods. 2021 Jul 16;10(7):1651. doi: 10.3390/foods10071651.