PMID- 34451254 OWN - NLM STAT- PubMed-not-MEDLINE LR - 20210831 IS - 2073-4360 (Electronic) IS - 2073-4360 (Linking) VI - 13 IP - 16 DP - 2021 Aug 13 TI - Visualization of Activated Area on Polymers for Evaluation of Atmospheric Pressure Plasma Jets. LID - 10.3390/polym13162711 [doi] LID - 2711 AB - The treatment of a polymer surface using an atmospheric pressure plasma jet (APPJ) causes a local increase of the surface free energy (SFE). The plasma-treated zone can be visualized with the use of a test ink and quantitatively evaluated. However, the inked area is shrinking with time. The shrinkage characteristics are collected using activation image recording (AIR). The recording is conducted by a digital camera. The physical mechanisms of activation area shrinkage are discussed. The error sources are analyzed and methods of error reduction are proposed. The standard deviation of the activation area is less than 3%. Three polymers, acrylonitrile butadiene styrene (ABS), high-density polyethylene (HDPE), and polyoxymethylene (POM), are examined as a test substrate material. Due to a wide variation range of SFE and a small hydrophobic recovery, HDPE is chosen. Since the chemical mixtures tend to temporal changes of the stoichiometry, the pure formamide test ink with 58 mN/m is selected. The method is tested for the characterization of five different types of discharge: (i) pulsed arc APPJ with the power of about 700 W; (ii) piezoelectric direct discharge APPJ; (iii) piezoelectric driven needle corona in ambient air; (iv) piezoelectric driven plasma needle in argon; and (v) piezoelectric driven dielectric barrier discharge (DBD). For piezoelectrically driven discharges, the power was either 4.5 W or 8 W. It is shown how the AIR method can be used to solve different engineering problems. FAU - Korzec, Dariusz AU - Korzec D AUID- ORCID: 0000-0002-6297-0163 AD - Relyon Plasma GmbH, Osterhofener Strasse 6, 93055 Regensburg, Germany. FAU - Andres, Thomas AU - Andres T AD - Relyon Plasma GmbH, Osterhofener Strasse 6, 93055 Regensburg, Germany. FAU - Brandes, Eva AU - Brandes E AD - Relyon Plasma GmbH, Osterhofener Strasse 6, 93055 Regensburg, Germany. FAU - Nettesheim, Stefan AU - Nettesheim S AD - Relyon Plasma GmbH, Osterhofener Strasse 6, 93055 Regensburg, Germany. LA - eng PT - Journal Article DEP - 20210813 PL - Switzerland TA - Polymers (Basel) JT - Polymers JID - 101545357 PMC - PMC8401304 OTO - NOTNLM OT - atmospheric pressure plasma jet OT - dielectric barrier discharge OT - piezoelectric direct discharge OT - surface activation OT - surface free energy OT - test ink COIS- The authors declare no conflict of interest. EDAT- 2021/08/29 06:00 MHDA- 2021/08/29 06:01 PMCR- 2021/08/13 CRDT- 2021/08/28 01:03 PHST- 2021/06/17 00:00 [received] PHST- 2021/07/30 00:00 [revised] PHST- 2021/08/08 00:00 [accepted] PHST- 2021/08/28 01:03 [entrez] PHST- 2021/08/29 06:00 [pubmed] PHST- 2021/08/29 06:01 [medline] PHST- 2021/08/13 00:00 [pmc-release] AID - polym13162711 [pii] AID - polymers-13-02711 [pii] AID - 10.3390/polym13162711 [doi] PST - epublish SO - Polymers (Basel). 2021 Aug 13;13(16):2711. doi: 10.3390/polym13162711.