PMID- 34832449 OWN - NLM STAT- PubMed-not-MEDLINE LR - 20211130 IS - 1996-1944 (Print) IS - 1996-1944 (Electronic) IS - 1996-1944 (Linking) VI - 14 IP - 22 DP - 2021 Nov 20 TI - Analysis of Selected Properties of Injection Moulded Sustainable Biocomposites from Poly(butylene succinate) and Wheat Bran. LID - 10.3390/ma14227049 [doi] LID - 7049 AB - The paper presents a procedure of the manufacturing and complex analysis of the properties of injection mouldings made of polymeric composites based on the poly(butylene succinate) (PBS) matrix with the addition of a natural filler in the form of wheat bran (WB). The scope of the research included measurements of processing shrinkage and density, analysis of the chemical structure, measurements of the thermal and thermo-mechanical properties (Differential Scanning Calorimetry (DSC) and Thermogravimetric Analysis (TG), Heat Deflection Temperature (HDT), and Vicat Softening Temperature (VST)), and measurements of the mechanical properties (hardness, impact strength, and static tensile test). The measurements were performed using design of experiment (DOE) methods, which made it possible to determine the investigated relationships in the form of polynomials and response surfaces. The mass content of the filler and the extruder screw speed during the production of the biocomposite granulate, which was used for the injection moulding of the test samples, constituted the variable factors adopted in the DOE. The study showed significant differences in the processing, thermal, and mechanical properties studied for individual systems of the DOE. FAU - Sasimowski, Emil AU - Sasimowski E AUID- ORCID: 0000-0003-0831-9967 AD - Department of Technology and Polymer Processing, Faculty of Mechanical Engineering, Lublin University of Technology, 20-618 Lublin, Poland. FAU - Majewski, Lukasz AU - Majewski L AUID- ORCID: 0000-0002-9766-2064 AD - Department of Technology and Polymer Processing, Faculty of Mechanical Engineering, Lublin University of Technology, 20-618 Lublin, Poland. FAU - Grochowicz, Marta AU - Grochowicz M AUID- ORCID: 0000-0002-9225-5232 AD - Department of Polymer Chemistry, Institute of Chemical Sciences, Faculty of Chemistry, Maria Curie-Sklodowska University, 20-400 Lublin, Poland. LA - eng GR - 030/RID/2018/19/Ministry of Science and Higher Education/ PT - Journal Article DEP - 20211120 PL - Switzerland TA - Materials (Basel) JT - Materials (Basel, Switzerland) JID - 101555929 PMC - PMC8623204 OTO - NOTNLM OT - agro-flour filler OT - agro-waste materials OT - biofiller OT - bioplastic OT - composite OT - injection moulding OT - mechanical properties OT - thermal properties OT - thermo-mechanical properties COIS- The authors declare no conflict of interest. The funders had no role in the design of the study; in the collection, analyses, or interpretation of data; in the writing of the manuscript; or in the decision to publish the results. EDAT- 2021/11/28 06:00 MHDA- 2021/11/28 06:01 PMCR- 2021/11/20 CRDT- 2021/11/27 01:18 PHST- 2021/10/25 00:00 [received] PHST- 2021/11/12 00:00 [revised] PHST- 2021/11/18 00:00 [accepted] PHST- 2021/11/27 01:18 [entrez] PHST- 2021/11/28 06:00 [pubmed] PHST- 2021/11/28 06:01 [medline] PHST- 2021/11/20 00:00 [pmc-release] AID - ma14227049 [pii] AID - materials-14-07049 [pii] AID - 10.3390/ma14227049 [doi] PST - epublish SO - Materials (Basel). 2021 Nov 20;14(22):7049. doi: 10.3390/ma14227049.