PMID- 35175888
OWN - NLM
STAT- MEDLINE
DCOM- 20231031
LR  - 20231031
IS  - 1547-6510 (Electronic)
IS  - 1040-8347 (Linking)
VI  - 53
IP  - 8
DP  - 2023
TI  - Critical Evaluation of Analytical Methods for the Determination of Anthropogenic 
      Organic Contaminants in Edible Oils: An Overview of the Last Five Years.
PG  - 1733-1747
LID - 10.1080/10408347.2022.2040352 [doi]
AB  - Anthropogenic contaminants, as pesticides, polycyclic aromatic hydrocarbons 
      (PAHs) and monochloropropanediols (MCPDs), have become important to be controlled 
      in edible oils, since their regular occurrence. In fact, alerts from the Rapid 
      Alert System for Food and Feed (RASFF) in oils normally include these compounds. 
      From a critical point of view, tools used to control these compounds in the last 
      5 years will be discussed, including sample preparation, analysis and current 
      regulations. Extraction and analysis methods will be discussed next, being 
      liquid-liquid extraction (LLE) and QuEChERS, with or without clean-up step, as 
      well as chromatographic methods coupled to different analyzers (mainly mass 
      spectrometry), the most commonly used for extraction and analysis respectively. 
      Occurrence in samples will also be reviewed and compared with the legal maximum 
      residue limits (MRLs), observing that 4%, 20% and 60% of the analyzed samples 
      exceed the legal limits for pesticides, MCPDs and PAHs respectively.
FAU - Lopez-Ruiz, Rosalia
AU  - Lopez-Ruiz R
AUID- ORCID: 0000-0003-0806-9013
AD  - Research Group "Analytical Chemistry of Contaminants", Department of Chemistry 
      and Physics, Research Centre for Mediterranean Intensive Agrosystems and 
      Agri-Food Biotechnology (CIAIMBITAL), Agrifood Campus of International 
      Excellence, University of Almeria, Almeria, Spain.
AD  - Laboratory of Pesticide Residue Analysis (LARP), Chemistry Department, Federal 
      University of Santa Maria, Santa Maria, RS, Brazil.
FAU - Marin-Saez, Jesus
AU  - Marin-Saez J
AUID- ORCID: 0000-0002-4153-9788
AD  - Research Group "Analytical Chemistry of Contaminants", Department of Chemistry 
      and Physics, Research Centre for Mediterranean Intensive Agrosystems and 
      Agri-Food Biotechnology (CIAIMBITAL), Agrifood Campus of International 
      Excellence, University of Almeria, Almeria, Spain.
FAU - Prestes, Osmar D
AU  - Prestes OD
AUID- ORCID: 0000-0002-6012-7172
AD  - Laboratory of Pesticide Residue Analysis (LARP), Chemistry Department, Federal 
      University of Santa Maria, Santa Maria, RS, Brazil.
FAU - Romero-Gonzalez, Roberto
AU  - Romero-Gonzalez R
AUID- ORCID: 0000-0002-2505-2056
AD  - Research Group "Analytical Chemistry of Contaminants", Department of Chemistry 
      and Physics, Research Centre for Mediterranean Intensive Agrosystems and 
      Agri-Food Biotechnology (CIAIMBITAL), Agrifood Campus of International 
      Excellence, University of Almeria, Almeria, Spain.
FAU - Garrido Frenich, Antonia
AU  - Garrido Frenich A
AUID- ORCID: 0000-0002-7904-7842
AD  - Research Group "Analytical Chemistry of Contaminants", Department of Chemistry 
      and Physics, Research Centre for Mediterranean Intensive Agrosystems and 
      Agri-Food Biotechnology (CIAIMBITAL), Agrifood Campus of International 
      Excellence, University of Almeria, Almeria, Spain.
LA  - eng
PT  - Journal Article
PT  - Review
DEP - 20220217
PL  - United States
TA  - Crit Rev Anal Chem
JT  - Critical reviews in analytical chemistry
JID - 9004784
RN  - 0 (Oils)
RN  - 0 (Polycyclic Aromatic Hydrocarbons)
RN  - 0 (Pesticides)
SB  - IM
MH  - Oils/chemistry
MH  - *Polycyclic Aromatic Hydrocarbons/analysis
MH  - Gas Chromatography-Mass Spectrometry/methods
MH  - Chromatography, High Pressure Liquid
MH  - *Pesticides/analysis
OTO - NOTNLM
OT  - Determination
OT  - LLE
OT  - MCPDs
OT  - PAHs
OT  - edible oils
OT  - pesticides
EDAT- 2022/02/18 06:00
MHDA- 2023/10/31 06:42
CRDT- 2022/02/17 17:13
PHST- 2023/10/31 06:42 [medline]
PHST- 2022/02/18 06:00 [pubmed]
PHST- 2022/02/17 17:13 [entrez]
AID - 10.1080/10408347.2022.2040352 [pii]
AID - 10.1080/10408347.2022.2040352 [doi]
PST - ppublish
SO  - Crit Rev Anal Chem. 2023;53(8):1733-1747. doi: 10.1080/10408347.2022.2040352. 
      Epub 2022 Feb 17.