PMID- 35492944
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20220716
IS  - 2046-2069 (Electronic)
IS  - 2046-2069 (Linking)
VI  - 10
IP  - 18
DP  - 2020 Mar 11
TI  - A simplified fabric phase sorptive extraction method for the determination of 
      amphetamine drugs in water samples using liquid chromatography-mass spectrometry.
PG  - 10854-10866
LID - 10.1039/c9ra10138a [doi]
AB  - Fabric phase sorptive extraction (FPSE) can directly extract the target analytes 
      and simultaneously determine many similar substances from complicated sample 
      matrices. Also, it has very high chemical stability. Therefore, we used fabric 
      phase sorptive extraction to analyze three amphetamine drugs (amphetamine (AM), 
      methamphetamine (MAM), and 3,4-methylenedioxymethamphetamine (MDMA)) in water. 
      This was coupled with ultrahigh-performance liquid chromatography and tandem mass 
      spectrometry. The effects of different sorbent chemistries such as sorption time, 
      ratios of back-extraction solvents, back-extraction time, and the salt effect on 
      the extraction efficiency were studied; the optimum operation conditions were 
      determined. Medium polarity polar polymer-coated FPSE media were created using 
      short-chain poly (tetrahydrofuran) (PTHF). This is the most efficient extraction 
      media for the analytes of interest. Under the optimized conditions, the linear 
      range of the three amphetamine drugs were 0.1-150.0 (AM, MAM) and 0.5-200 ng 
      mL(-1) (MDMA). The correlation coefficients (gamma) were 0.9947 (AM), 0.9925 (MAM), 
      and 0.9918 (MDMA). The detection limits (LOD) were 0.025 ng mL(-1) for AM, 0.029 
      ng mL(-1) for MAM, and 0.01 ng mL(-1) for MDMA. The corresponding limit of 
      quantification values (LOQ) were 0.083 ng mL(-1), 0.097 ng mL(-1), and 0.031 ng 
      mL(-1), respectively. The recoveries were 73.4-91.6%, 82.6-95.4%, and 92.7-95.3%, 
      respectively, and the relative standard deviations (RSD) were 1.65-6.88%, 
      1.38-6.11%, and 1.58-7.34%, respectively. Moreover, our method can be 
      successfully applied for the analysis of amphetamines in wastewater samples, and 
      at the same time, lays the foundation for the future detection of such 
      substances.
CI  - This journal is (c) The Royal Society of Chemistry.
FAU - Ruan, Xiaomeng
AU  - Ruan X
AD  - Criminal Investigation Police University of China China xinglimei1@sina.com +86 
      13898164819.
FAU - Xing, Limei
AU  - Xing L
AUID- ORCID: 0000-0002-8099-9138
AD  - Criminal Investigation Police University of China China xinglimei1@sina.com +86 
      13898164819.
FAU - Peng, Ju
AU  - Peng J
AD  - Criminal Investigation Police University of China China xinglimei1@sina.com +86 
      13898164819.
FAU - Li, Shiying
AU  - Li S
AD  - Criminal Investigation Police University of China China xinglimei1@sina.com +86 
      13898164819.
FAU - Song, Yiqun
AU  - Song Y
AD  - Criminal Investigation Police University of China China xinglimei1@sina.com +86 
      13898164819.
FAU - Sun, Qianqian
AU  - Sun Q
AD  - Criminal Investigation Police University of China China xinglimei1@sina.com +86 
      13898164819.
LA  - eng
PT  - Journal Article
DEP - 20200317
PL  - England
TA  - RSC Adv
JT  - RSC advances
JID - 101581657
PMC - PMC9050397
COIS- We declare that we do not have any commercial or associative interest that 
      represents a conflict of interest in connection with the work submitted.
EDAT- 2020/03/17 00:00
MHDA- 2020/03/17 00:01
PMCR- 2020/03/17
CRDT- 2022/05/02 06:15
PHST- 2019/12/04 00:00 [received]
PHST- 2020/02/03 00:00 [accepted]
PHST- 2022/05/02 06:15 [entrez]
PHST- 2020/03/17 00:00 [pubmed]
PHST- 2020/03/17 00:01 [medline]
PHST- 2020/03/17 00:00 [pmc-release]
AID - c9ra10138a [pii]
AID - 10.1039/c9ra10138a [doi]
PST - epublish
SO  - RSC Adv. 2020 Mar 17;10(18):10854-10866. doi: 10.1039/c9ra10138a. eCollection 
      2020 Mar 11.