PMID- 35519781
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20220507
IS  - 2046-2069 (Electronic)
IS  - 2046-2069 (Linking)
VI  - 10
IP  - 44
DP  - 2020 Jul 9
TI  - Amorphous mesostructured zirconia with high (hydro)thermal stability.
PG  - 26165-26176
LID - 10.1039/d0ra04824k [doi]
AB  - Here, combining the evaporation-induced self-assembly (EISA) method and the 
      liquid crystal templating pathway, mesostructured amorphous zirconium oxides have 
      been prepared by a soft templating method without addition of any heteroelement 
      to stabilize the mesopore framework. The recovered materials have been 
      characterized by SAXS measurements, nitrogen adsorption-desorption analysis and 
      X-ray diffraction (XRD). The obtained mesostructured zirconia exhibits a high 
      thermal stability. An in situ XRD study performed as a function of temperature 
      shows that the amorphous ZrO(2), obtained after removal of the pore templating 
      agent (pluronic P123), begins to crystallize in air from 420  degrees C. Amorphous 
      mesostructured ZrO(2) also presents a high hydrothermal stability; these 
      materials are not degraded after 72 hours in boiling water.
CI  - This journal is (c) The Royal Society of Chemistry.
FAU - Lebeau, Benedicte
AU  - Lebeau B
AD  - Universite de Haute Alsace (UHA), CNRS, IS2M UMR 7361 F-68100 Mulhouse France.
AD  - Universite de Strasbourg 67000 Strasbourg France.
FAU - Naboulsi, Issam
AU  - Naboulsi I
AD  - Universite de Lorraine, CNRS, L2CM 7053, Faculte des Sciences et Technologies BP 
      70239 F-54506 Vandoeuvre-les-Nancy Cedex France Jean-Luc.Blin@univ-lorraine.fr 
      +33 3 83 68 43 70.
FAU - Michelin, Laure
AU  - Michelin L
AD  - Universite de Haute Alsace (UHA), CNRS, IS2M UMR 7361 F-68100 Mulhouse France.
AD  - Universite de Strasbourg 67000 Strasbourg France.
FAU - Marichal, Claire
AU  - Marichal C
AD  - Universite de Haute Alsace (UHA), CNRS, IS2M UMR 7361 F-68100 Mulhouse France.
AD  - Universite de Strasbourg 67000 Strasbourg France.
FAU - Rigolet, Severinne
AU  - Rigolet S
AD  - Universite de Haute Alsace (UHA), CNRS, IS2M UMR 7361 F-68100 Mulhouse France.
AD  - Universite de Strasbourg 67000 Strasbourg France.
FAU - Carteret, Cedric
AU  - Carteret C
AD  - Universite de Lorraine, CNRS, LCPME F-54000 Nancy France.
FAU - Brunet, Sylvette
AU  - Brunet S
AD  - Universite de Poitiers, CNRS, IC2MP, UMR 7285 86073 Poitiers Cedex 9 France.
FAU - Bonne, Magali
AU  - Bonne M
AUID- ORCID: 0000-0003-0417-6567
AD  - Universite de Haute Alsace (UHA), CNRS, IS2M UMR 7361 F-68100 Mulhouse France.
AD  - Universite de Strasbourg 67000 Strasbourg France.
FAU - Blin, Jean-Luc
AU  - Blin JL
AUID- ORCID: 0000-0002-0947-2552
AD  - Universite de Lorraine, CNRS, L2CM 7053, Faculte des Sciences et Technologies BP 
      70239 F-54506 Vandoeuvre-les-Nancy Cedex France Jean-Luc.Blin@univ-lorraine.fr 
      +33 3 83 68 43 70.
LA  - eng
PT  - Journal Article
DEP - 20200713
PL  - England
TA  - RSC Adv
JT  - RSC advances
JID - 101581657
PMC - PMC9055362
COIS- There are no conflicts to declare.
EDAT- 2020/07/13 00:00
MHDA- 2020/07/13 00:01
PMCR- 2020/07/13
CRDT- 2022/05/06 06:07
PHST- 2020/06/01 00:00 [received]
PHST- 2020/07/07 00:00 [accepted]
PHST- 2022/05/06 06:07 [entrez]
PHST- 2020/07/13 00:00 [pubmed]
PHST- 2020/07/13 00:01 [medline]
PHST- 2020/07/13 00:00 [pmc-release]
AID - d0ra04824k [pii]
AID - 10.1039/d0ra04824k [doi]
PST - epublish
SO  - RSC Adv. 2020 Jul 13;10(44):26165-26176. doi: 10.1039/d0ra04824k. eCollection 
      2020 Jul 9.