PMID- 35521266
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20231103
IS  - 2046-2069 (Electronic)
IS  - 2046-2069 (Linking)
VI  - 10
IP  - 61
DP  - 2020 Oct 7
TI  - Simultaneous determination of 11 antiseptic ingredients in surface water based on 
      polypyrrole decorated magnetic nanoparticles.
PG  - 37473-37481
LID - 10.1039/d0ra07064e [doi]
AB  - With the emergence and spread of coronavirus COVID-19, the use of personal 
      cleansing, medical and household disinfectant products have increased 
      significantly. In this work, a new magnetic solid-phase extraction (MSPE) method 
      for the determination of 11 antiseptic ingredients in surface water by high 
      performance liquid chromatography-mass spectrometry (HPLC-MS/MS) for 6 months 
      based on Fe(3)O(4)@PPy magnetic nanoparticles (MNPs) was established. The MSPE 
      method possessed the advantages of simple processing, little time consumption and 
      less organic solvent consumption, and the MNPs could be reused several times. The 
      analytical parameters influencing the extraction efficiency, such as sample pH, 
      amount of MNPs and extraction time, were optimized in detail. It was indicated 
      that the method had satisfactory linearities in the range of 0.50 to 1000.0 mug 
      L(-1) with the correlation coefficients (r) higher than 0.9996. Additionally, 
      satisfactory spiked recoveries were achieved in the range of 80.21-107.33% with 
      relative standard deviations (RSDs) from 1.98% to 8.05%. The limits of detection 
      (LODs) and limits of quantitation (LOQs) were in the range of 0.20 to 2.0 mug 
      L(-1) and 0.50 to 5.0 mug L(-1). Therefore, the developed MSPE-HPLC-MS/MS method 
      has high selectivity and stability, and satisfactory quantitative capability for 
      the antiseptic ingredients in surface water. Furthermore, this method can provide 
      relevant technical support for the development of surface water standards.
CI  - This journal is (c) The Royal Society of Chemistry.
FAU - Zhang, Mengyan
AU  - Zhang M
AD  - Hebei Key Laboratory of Environment and Human Health, School of Public Health, 
      Hebei Medical University Shijiazhuang 050017 PR China kangwj158@163.com 
      tangjuan2002@163.com.
FAU - Lian, Kaoqi
AU  - Lian K
AUID- ORCID: 0000-0003-4876-2568
AD  - Hebei Key Laboratory of Environment and Human Health, School of Public Health, 
      Hebei Medical University Shijiazhuang 050017 PR China kangwj158@163.com 
      tangjuan2002@163.com.
FAU - Ai, Lianfeng
AU  - Ai L
AD  - Technology Center of Shijiazhuang Customs Shijiazhuang 050051 China.
FAU - Kang, Weijun
AU  - Kang W
AUID- ORCID: 0000-0003-2431-5990
AD  - Hebei Key Laboratory of Environment and Human Health, School of Public Health, 
      Hebei Medical University Shijiazhuang 050017 PR China kangwj158@163.com 
      tangjuan2002@163.com.
FAU - Zhao, Tangjuan
AU  - Zhao T
AD  - Hebei Key Laboratory of Environment and Human Health, School of Public Health, 
      Hebei Medical University Shijiazhuang 050017 PR China kangwj158@163.com 
      tangjuan2002@163.com.
LA  - eng
PT  - Journal Article
DEP - 20201012
PL  - England
TA  - RSC Adv
JT  - RSC advances
JID - 101581657
PMC - PMC9057185
COIS- There are no conflicts to declare.
EDAT- 2020/10/12 00:00
MHDA- 2020/10/12 00:01
PMCR- 2020/10/12
CRDT- 2022/05/06 06:18
PHST- 2020/08/17 00:00 [received]
PHST- 2020/09/29 00:00 [accepted]
PHST- 2022/05/06 06:18 [entrez]
PHST- 2020/10/12 00:00 [pubmed]
PHST- 2020/10/12 00:01 [medline]
PHST- 2020/10/12 00:00 [pmc-release]
AID - d0ra07064e [pii]
AID - 10.1039/d0ra07064e [doi]
PST - epublish
SO  - RSC Adv. 2020 Oct 12;10(61):37473-37481. doi: 10.1039/d0ra07064e. eCollection 
      2020 Oct 7.