PMID- 35530671
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20231103
IS  - 2046-2069 (Electronic)
IS  - 2046-2069 (Linking)
VI  - 9
IP  - 60
DP  - 2019 Oct 28
TI  - A bromine-catalysis-synthesized poly(3,4-ethylenedioxythiophene)/graphitic carbon 
      nitride electrochemical sensor for heavy metal ion determination.
PG  - 34691-34698
LID - 10.1039/c9ra02161b [doi]
AB  - In this paper, poly(3,4-ethylenedioxythiophene)/graphitic carbon nitride 
      (PEDOT/g-C(3)N(4)) composites were prepared by the bromine catalysed 
      polymerization (BCP) method with varying weight ratios of monomer to g-C(3)N(4). 
      For comparison, solid-state polymerization (SSP) and metal oxidative 
      polymerization (MOP) methods were also used for the synthesis of PEDOT/g-C(3)N(4) 
      composites. Electrochemical determination of heavy metal ions (Cd(2+) and Pb(2+)) 
      was carried out by differential pulse voltammetry (DPV) on composite-modified 
      glass carbon electrodes (GCEs), which were prepared by different methods. The 
      obtained composites were analysed by Fourier transform infrared spectroscopy 
      (FT-IR), ultraviolet-visible absorption spectroscopy (UV-vis), X-ray diffraction 
      (XRD), energy-dispersive X-ray spectroscopy (EDS), scanning electron microscopy 
      (SEM), and transmission electron microscopy (TEM). The results showed that the 
      bromine catalysed polymerization (BCP) method is an effective way to prepare the 
      PEDOT/g-C(3)N(4) composite, and the combination of PEDOT with g-C(3)N(4) can 
      improve the electrochemical activity of electrode materials. And, the composite 
      from the BCP method modified electrode (PEDOT/10 wt% g-C(3)N(4)/GCE) exhibited 
      the widest linear responses for Cd(2+) and Pb(2+), ranging from 0.06-12 muM and 
      0.04-11.6 muM with detection limits (S/N = 3) of 0.0014 muM and 0.00421 muM, 
      respectively.
CI  - This journal is (c) The Royal Society of Chemistry.
FAU - Wu, Wei
AU  - Wu W
AD  - Key Laboratory of Oil and Gas Fine Chemicals, Ministry of Education, Xinjiang 
      Uygur Autonomous Region, Xinjiang University Urumqi 830046 P. R. China 
      tursunabdir@sina.com.cn jruxangul@sina.com.
AD  - Key Laboratory of Functional Polymers, Xinjiang University Urumqi 830046 People's 
      Republic of China.
FAU - Ali, Ahmat
AU  - Ali A
AD  - Key Laboratory of Oil and Gas Fine Chemicals, Ministry of Education, Xinjiang 
      Uygur Autonomous Region, Xinjiang University Urumqi 830046 P. R. China 
      tursunabdir@sina.com.cn jruxangul@sina.com.
AD  - Key Laboratory of Functional Polymers, Xinjiang University Urumqi 830046 People's 
      Republic of China.
FAU - Jamal, Ruxangul
AU  - Jamal R
AD  - Key Laboratory of Oil and Gas Fine Chemicals, Ministry of Education, Xinjiang 
      Uygur Autonomous Region, Xinjiang University Urumqi 830046 P. R. China 
      tursunabdir@sina.com.cn jruxangul@sina.com.
AD  - Key Laboratory of Functional Polymers, Xinjiang University Urumqi 830046 People's 
      Republic of China.
FAU - Abdulla, Mihray
AU  - Abdulla M
AD  - Key Laboratory of Oil and Gas Fine Chemicals, Ministry of Education, Xinjiang 
      Uygur Autonomous Region, Xinjiang University Urumqi 830046 P. R. China 
      tursunabdir@sina.com.cn jruxangul@sina.com.
AD  - Key Laboratory of Functional Polymers, Xinjiang University Urumqi 830046 People's 
      Republic of China.
FAU - Bakri, Tursunnisahan
AU  - Bakri T
AD  - Key Laboratory of Oil and Gas Fine Chemicals, Ministry of Education, Xinjiang 
      Uygur Autonomous Region, Xinjiang University Urumqi 830046 P. R. China 
      tursunabdir@sina.com.cn jruxangul@sina.com.
AD  - Key Laboratory of Functional Polymers, Xinjiang University Urumqi 830046 People's 
      Republic of China.
FAU - Abdiryim, Tursun
AU  - Abdiryim T
AUID- ORCID: 0000-0003-3828-7986
AD  - Key Laboratory of Oil and Gas Fine Chemicals, Ministry of Education, Xinjiang 
      Uygur Autonomous Region, Xinjiang University Urumqi 830046 P. R. China 
      tursunabdir@sina.com.cn jruxangul@sina.com.
AD  - Key Laboratory of Functional Polymers, Xinjiang University Urumqi 830046 People's 
      Republic of China.
LA  - eng
PT  - Journal Article
DEP - 20191028
PL  - England
TA  - RSC Adv
JT  - RSC advances
JID - 101581657
PMC - PMC9073917
COIS- There are no conflicts to declare.
EDAT- 2019/10/28 00:00
MHDA- 2019/10/28 00:01
PMCR- 2019/10/28
CRDT- 2022/05/09 04:25
PHST- 2019/03/20 00:00 [received]
PHST- 2019/10/21 00:00 [accepted]
PHST- 2022/05/09 04:25 [entrez]
PHST- 2019/10/28 00:00 [pubmed]
PHST- 2019/10/28 00:01 [medline]
PHST- 2019/10/28 00:00 [pmc-release]
AID - c9ra02161b [pii]
AID - 10.1039/c9ra02161b [doi]
PST - epublish
SO  - RSC Adv. 2019 Oct 28;9(60):34691-34698. doi: 10.1039/c9ra02161b. eCollection 2019 
      Oct 28.