PMID- 35539276
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20220512
IS  - 2046-2069 (Electronic)
IS  - 2046-2069 (Linking)
VI  - 8
IP  - 31
DP  - 2018 May 9
TI  - Fast quantification of fluoroquinolones in environmental water samples using 
      molecularly imprinted polymers coupled with internal extractive electrospray 
      ionization mass spectrometry.
PG  - 17293-17299
LID - 10.1039/c8ra01837e [doi]
AB  - In this study, a facile method based on molecularly imprinted polymers (MIPs) 
      combined with internal extractive electrospray ionization tandem mass 
      spectrometry (iEESI-MS/MS) was developed for the quantitative analysis of 
      fluoroquinolones (FQs) in environmental water samples. FQ molecules in water 
      samples were captured by the MIPs, which was retained on a 0.22 mum syringe 
      filter. Then, an electrospray solution selected as the elution solution was 
      employed to extract the FQs from the MIPs, getting an eluate of FQs for mass 
      spectrometric interrogation. Under the optimized experimental conditions, low 
      limits of detection (LODs, 0.015-0.026 mug L(-1)), with relative standard 
      deviations (RSDs) less than 8.81% (n = 6) were obtained. The present method also 
      provides good recoveries (91.14-103.60%) with acceptable precision (RSDs < 6.18%) 
      and have no serious matrix effects for environmental water samples. The 
      experimental results demonstrated that MIPs-iEESI-MS/MS has advantages including 
      easy use, high speed (less than 3 min per sample) and high sensitivity for the 
      analysis of FQs in environmental water samples, showing potential application in 
      environmental science and water safety control.
CI  - This journal is (c) The Royal Society of Chemistry.
FAU - Kou, Wei
AU  - Kou W
AD  - State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of 
      Chemistry, Jilin University Changchun 130012 China.
FAU - Zhang, Hua
AU  - Zhang H
AUID- ORCID: 0000-0003-2875-7243
AD  - State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of 
      Chemistry, Jilin University Changchun 130012 China.
FAU - Bibi, Aisha
AU  - Bibi A
AUID- ORCID: 0000-0003-3729-5941
AD  - State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of 
      Chemistry, Jilin University Changchun 130012 China.
FAU - Ke, Mufang
AU  - Ke M
AD  - State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of 
      Chemistry, Jilin University Changchun 130012 China.
FAU - Han, Jing
AU  - Han J
AD  - State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of 
      Chemistry, Jilin University Changchun 130012 China.
FAU - Xiong, Jianliang
AU  - Xiong J
AUID- ORCID: 0000-0002-0669-4168
AD  - School of Pharmaceutical Sciences, Peking University Beijing 100191 China.
FAU - Su, Rui
AU  - Su R
AUID- ORCID: 0000-0001-7567-6361
AD  - State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of 
      Chemistry, Jilin University Changchun 130012 China.
AD  - Changchun University of Chinese Medicine Changchun 130117 China 
      sranalchem@163.com.
FAU - Liang, Dapeng
AU  - Liang D
AD  - State Key Lab of Groundwater Resources and Environment Ministry of Education, 
      Jilin University Changchun 130012 China liangdp@jlu.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20180511
PL  - England
TA  - RSC Adv
JT  - RSC advances
JID - 101581657
PMC - PMC9080410
COIS- The authors declare that the research was conducted in the absence of any 
      commercial or financial relationships that could be construed as a potential 
      conflict of interest.
EDAT- 2018/05/11 00:00
MHDA- 2018/05/11 00:01
PMCR- 2018/05/11
CRDT- 2022/05/11 03:47
PHST- 2018/03/02 00:00 [received]
PHST- 2018/04/22 00:00 [accepted]
PHST- 2022/05/11 03:47 [entrez]
PHST- 2018/05/11 00:00 [pubmed]
PHST- 2018/05/11 00:01 [medline]
PHST- 2018/05/11 00:00 [pmc-release]
AID - c8ra01837e [pii]
AID - 10.1039/c8ra01837e [doi]
PST - epublish
SO  - RSC Adv. 2018 May 11;8(31):17293-17299. doi: 10.1039/c8ra01837e. eCollection 2018 
      May 9.