PMID- 35683271 OWN - NLM STAT- PubMed-not-MEDLINE LR - 20220716 IS - 1996-1944 (Print) IS - 1996-1944 (Electronic) IS - 1996-1944 (Linking) VI - 15 IP - 11 DP - 2022 Jun 2 TI - The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel. LID - 10.3390/ma15113970 [doi] LID - 3970 AB - To further improve the mechanical properties of H13 steel at room and high temperatures, its precipitates were regulated based on the Thermo-Calc results. Scanning electron microscope (SEM), electron backscattering diffraction (EBSD), transmission electron microscope (TEM), and X-ray diffraction (XRD) Rietveld refinement were used to study the effect of the intercritical annealing on the microstructure and mechanical properties of H13 steel. The results show that the intercritical annealing at 850~95 degrees C increased the VC volume fraction from 2.23 to 3.03~3.48%. Increasing the VC volume fraction could inhibit the M(7)C(3) precipitation from 10.01 to 6.63~5.72% during tempering. A large amount of VC also promoted the M(23)C(6) precipitation during tempering at higher dislocation densities. The intercortical annealing simultaneously increased the elongation of H13 steel. An excellent combination (room temperature: ultimate tensile strength (UTS) of 898 MPa and total elongation (TEL) of 19.35%, 650 degrees C: UTS of 439 MPa, and TEL of 27.80%) could be obtained when intercritical annealing is performed at 900 degrees C. Meanwhile, after aging at 650 degrees C for 128 h, the room temperature UTS and TEL decreased by only 31 MPa and 0.52%, respectively. FAU - Shi, Kefei AU - Shi K AD - College of Materials and Metallurgy, Guizhou University, Guiyang 550025, China. AD - Key Laboratory for Materials Structure and Strength of Guizhou Province, Guizhou University, Huaxi District, Guiyang 550025, China. FAU - Zhao, Fei AU - Zhao F AD - College of Materials and Metallurgy, Guizhou University, Guiyang 550025, China. AD - Key Laboratory for Materials Structure and Strength of Guizhou Province, Guizhou University, Huaxi District, Guiyang 550025, China. FAU - Liu, Yuan AU - Liu Y AD - College of Materials and Metallurgy, Guizhou University, Guiyang 550025, China. AD - Key Laboratory for Materials Structure and Strength of Guizhou Province, Guizhou University, Huaxi District, Guiyang 550025, China. FAU - Yin, Sheng AU - Yin S AD - College of Materials and Metallurgy, Guizhou University, Guiyang 550025, China. AD - Key Laboratory for Materials Structure and Strength of Guizhou Province, Guizhou University, Huaxi District, Guiyang 550025, China. FAU - Yang, Ronggui AU - Yang R AD - College of Materials and Metallurgy, Guizhou University, Guiyang 550025, China. AD - Key Laboratory for Materials Structure and Strength of Guizhou Province, Guizhou University, Huaxi District, Guiyang 550025, China. LA - eng GR - No. QKHZX2022023/Science and Technology Fund of Guizhou Province/ GR - No. 51571066/National Natural Science Foundation of China/ GR - No. 20165654/Hundred-level Innovative Talents Project of Guizhou Province/ GR - No. 20194011/Central Government Guides Local Science and Technology Development Special Project/ PT - Journal Article DEP - 20220602 PL - Switzerland TA - Materials (Basel) JT - Materials (Basel, Switzerland) JID - 101555929 PMC - PMC9181995 OTO - NOTNLM OT - H13 steel OT - carbide OT - high temperature OT - intercritical annealing OT - precipitation COIS- The authors declare that they have no known competing financial interest or personal relationships that could have appeared to influence the work reported in this paper. EDAT- 2022/06/11 06:00 MHDA- 2022/06/11 06:01 PMCR- 2022/06/02 CRDT- 2022/06/10 01:17 PHST- 2022/04/28 00:00 [received] PHST- 2022/05/25 00:00 [revised] PHST- 2022/06/01 00:00 [accepted] PHST- 2022/06/10 01:17 [entrez] PHST- 2022/06/11 06:00 [pubmed] PHST- 2022/06/11 06:01 [medline] PHST- 2022/06/02 00:00 [pmc-release] AID - ma15113970 [pii] AID - materials-15-03970 [pii] AID - 10.3390/ma15113970 [doi] PST - epublish SO - Materials (Basel). 2022 Jun 2;15(11):3970. doi: 10.3390/ma15113970.