PMID- 35868699
OWN - NLM
STAT- MEDLINE
DCOM- 20220726
LR  - 20220726
IS  - 1873-4324 (Electronic)
IS  - 0003-2670 (Linking)
VI  - 1220
DP  - 2022 Aug 8
TI  - SPR-based assay kit for rapid determination of Pb(2).
PG  - 340030
LID - S0003-2670(22)00601-8 [pii]
LID - 10.1016/j.aca.2022.340030 [doi]
AB  - A recyclable optical nanosensor was developed by immobilizing l-tyrosine 
      functionalized silver nanoparticles (AgNPs) on the polyethylene terephthalate 
      (PET) substrate for rapid determination of Pb(2+) ions. At first, the l-tyrosine 
      functionalized AgNPs were assessed in the solution phase; the response time was 
      lower than 15 s, and a limit of detection lower than 9 nM was obtained in the 
      dynamic range of 1-1000 nM. For fabrication of the optical assay kit, the design 
      of experiment (DOE) was used to optimize the immobilization efficiency of the 
      nanoparticles on PET films by studying AgNO(3) concentration and pH as two 
      crucial parameters. The assay kit in optimal conditions showed a sharp localized 
      surface plasmon resonance band suitable for sensitive determination of Pb(2+). 
      The fabricated sensor showed promising results for rapid determination of lead 
      ions with the limit of detection value as low as 1 nM (S/N = 3). The sensor 
      reproduced the obtained results even after three consecutive runs, which proved 
      the recyclability of the optical assay kit. The recoveries of the spiked 
      concentration in real samples were in the range of 95%-103%, which confirmed the 
      applicability of the sensor in practical applications.
CI  - Copyright (c) 2022 Elsevier B.V. All rights reserved.
FAU - Amirjani, Amirmostafa
AU  - Amirjani A
AD  - Department of Materials Science and Engineering, Sharif University of Technology, 
      P.O.Box: 11155-9466, Tehran, Iran. Electronic address: amirjani@sharif.edu.
FAU - Kamani, Paria
AU  - Kamani P
AD  - Department of Materials Science and Engineering, Sharif University of Technology, 
      P.O.Box: 11155-9466, Tehran, Iran.
FAU - Hosseini, Hamid Reza Madaah
AU  - Hosseini HRM
AD  - Department of Materials Science and Engineering, Sharif University of Technology, 
      P.O.Box: 11155-9466, Tehran, Iran. Electronic address: madaah@sharif.edu.
FAU - Sadrnezhaad, S K
AU  - Sadrnezhaad SK
AD  - Department of Materials Science and Engineering, Sharif University of Technology, 
      P.O.Box: 11155-9466, Tehran, Iran. Electronic address: sadrnezh@sharif.edu.
LA  - eng
PT  - Journal Article
DEP - 20220609
PL  - Netherlands
TA  - Anal Chim Acta
JT  - Analytica chimica acta
JID - 0370534
RN  - 0 (Ions)
RN  - 2P299V784P (Lead)
RN  - 3M4G523W1G (Silver)
RN  - 42HK56048U (Tyrosine)
SB  - IM
MH  - Ions
MH  - Lead
MH  - *Metal Nanoparticles
MH  - *Silver
MH  - Surface Plasmon Resonance/methods
MH  - Tyrosine
OTO - NOTNLM
OT  - Amino acid
OT  - Heavy metal
OT  - Lead ion
OT  - Nanosensor
OT  - Optical sensors
OT  - Plasmonic
OT  - Silver nanoparticles
OT  - l-tyrosine
EDAT- 2022/07/23 06:00
MHDA- 2022/07/27 06:00
CRDT- 2022/07/22 21:04
PHST- 2022/02/02 00:00 [received]
PHST- 2022/06/01 00:00 [revised]
PHST- 2022/06/02 00:00 [accepted]
PHST- 2022/07/22 21:04 [entrez]
PHST- 2022/07/23 06:00 [pubmed]
PHST- 2022/07/27 06:00 [medline]
AID - S0003-2670(22)00601-8 [pii]
AID - 10.1016/j.aca.2022.340030 [doi]
PST - ppublish
SO  - Anal Chim Acta. 2022 Aug 8;1220:340030. doi: 10.1016/j.aca.2022.340030. Epub 2022 
      Jun 9.