PMID- 35905684
OWN - NLM
STAT- MEDLINE
DCOM- 20220816
LR  - 20220816
IS  - 1873-3778 (Electronic)
IS  - 0021-9673 (Linking)
VI  - 1678
DP  - 2022 Aug 16
TI  - Simultaneous capture of hydrophilic and hydrophobic compounds from complex plants 
      by biosurfactant-assisted mechanical amorphous dispersion extraction.
PG  - 463356
LID - S0021-9673(22)00549-0 [pii]
LID - 10.1016/j.chroma.2022.463356 [doi]
AB  - A biosurfactant-assisted mechanical amorphous dispersion extraction (BA-MADE) 
      procedure was established for the simultaneous capture of hydrophilic phenolic 
      acids and hydrophobic tanshinones from Salvia miltiorrhiza. Single-factor 
      experiments and the response surface methodology were used to optimize and 
      analyze the crucial parameters for the method, such as the type and amount of 
      amorphous-dispersion extractants, grinding time, extraction time and 
      solid-to-liquid ratio. The optimized parameter values for the BA-MADE process 
      were 407.02 mg of sodium chenodeoxycholate, a grinding time of 4.87 min, an 
      extraction time of 4.92 min, and a solid-to-liquid ratio of 0.5:10 g/mL. The 
      calibration curves of danshensu, rosmarinic acid, lithospermic acid, salvianolic 
      acid B, salvianolic acid A, dihydrotanshinone I, cryptotanshinone, tanshinone I, 
      and tanshinone II A exhibited good linearity in the range of 1-500 mug/mL (R(2) >/= 
      0.9990). The limits of detection of nine analytes ranged from 5.46 to 130 ng/mL, 
      the relative standard deviations (RSDs) of intraday and interday precision were 
      less than 1.95 and 3.56%, respectively, and the recoveries of the real sample 
      were in the range of 85-113%, with RSD% below 3.21%. The BA-MADE method was 
      compared with previously reported methods, such as heating reflux extraction, 
      ultrasonic extraction and microwave-assisted micellar extraction, and the results 
      demonstrated that the developed method has significant advantages in the 
      simultaneous extraction of hydrophilic and hydrophobic active components from 
      Salvia miltiorrhiza.
CI  - Copyright (c) 2022 Elsevier B.V. All rights reserved.
FAU - Zhu, Si-Chen
AU  - Zhu SC
AD  - College of Material Chemistry and Chemical Engineering, Hangzhou Normal 
      University, Hangzhou 311121, China.
FAU - Shi, Min-Zhen
AU  - Shi MZ
AD  - College of Material Chemistry and Chemical Engineering, Hangzhou Normal 
      University, Hangzhou 311121, China.
FAU - Yu, Ya-Ling
AU  - Yu YL
AD  - College of Material Chemistry and Chemical Engineering, Hangzhou Normal 
      University, Hangzhou 311121, China.
FAU - Liu, Xun-Gao
AU  - Liu XG
AD  - College of Material Chemistry and Chemical Engineering, Hangzhou Normal 
      University, Hangzhou 311121, China.
FAU - Cao, Jun
AU  - Cao J
AD  - College of Material Chemistry and Chemical Engineering, Hangzhou Normal 
      University, Hangzhou 311121, China. Electronic address: caoj@hznu.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20220721
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Furans)
RN  - 0 (Phenanthrenes)
RN  - 0 (Quinones)
RN  - 562G9360V6 (dihydrotanshinone I)
SB  - IM
MH  - Chromatography, High Pressure Liquid/methods
MH  - Furans
MH  - Phenanthrenes
MH  - Quinones
MH  - *Salvia miltiorrhiza/chemistry
OTO - NOTNLM
OT  - Biosurfactant
OT  - Hydrophilic phenolic acids
OT  - Hydrophobic tanshinones
OT  - Mechanical amorphous dispersion extraction
OT  - Response surface methodology
COIS- Declaration of Competing Interest We declare that we have no financial and 
      personal relationships with other people or organizations that can 
      inappropriately influence our work, there is no professional or other personal 
      interest of any nature or kind in any product, service and/or company that could 
      be construed as influencing the position presented in, or the review of, the 
      manuscript entitled, "Simultaneous capture of hydrophilic and hydrophobic 
      compounds from complex plants by biosurfactant-assisted mechanical amorphous 
      dispersion extraction".
EDAT- 2022/07/30 06:00
MHDA- 2022/08/17 06:00
CRDT- 2022/07/29 18:25
PHST- 2022/05/08 00:00 [received]
PHST- 2022/06/24 00:00 [revised]
PHST- 2022/07/19 00:00 [accepted]
PHST- 2022/07/30 06:00 [pubmed]
PHST- 2022/08/17 06:00 [medline]
PHST- 2022/07/29 18:25 [entrez]
AID - S0021-9673(22)00549-0 [pii]
AID - 10.1016/j.chroma.2022.463356 [doi]
PST - ppublish
SO  - J Chromatogr A. 2022 Aug 16;1678:463356. doi: 10.1016/j.chroma.2022.463356. Epub 
      2022 Jul 21.