PMID- 36298130 OWN - NLM STAT- MEDLINE DCOM- 20221028 LR - 20221030 IS - 1424-8220 (Electronic) IS - 1424-8220 (Linking) VI - 22 IP - 20 DP - 2022 Oct 13 TI - Electrochemical Determination of Morin in Natural Food Using a Chitosan-Graphene Glassy Carbon Modified Electrode. LID - 10.3390/s22207780 [doi] LID - 7780 AB - This report presents a new application for the chitosan-graphene glassy carbon electrode (Ch-G/GCE) system in the determination of the hydroxyflavonoid morin (MR), one of the flavonoids with the highest favorable activity for people, due to its natural properties by square-wave voltammetry (SWV). The anodic peak current for MR was observed at 0.50 V with an increase of 73% compared with the glassy carbon electrode unmodified. The surface areas of Ch-G/GCE, Ch/GCE and GCE evaluated by cyclic voltammetry were 0.140, 0.053 and 0.011 cm(2), respectively. Additionally, an increase greater than 100% compared to the electrode without modification was observed. The detection limit was 0.30 micromol/L for MR, and the relative standard deviations (RSDs) were 1.8% (n = 6). Possible interferences as quercetin, rutin, and applications in real samples were also evaluated with very acceptable results. FAU - Nagles, Edgar AU - Nagles E AD - Facultad de Quimica e Ingenieria Quimica, Universidad Nacional Mayor de San Marcos, Lima 15081, Peru. FAU - Bello, Monica AU - Bello M AD - Facultad de Ciencias Naturales y Matematicas, Universidad Nacional Federico Villareal, Lima 15001, Peru. FAU - Hurtado, John J AU - Hurtado JJ AUID- ORCID: 0000-0002-0511-9719 AD - Departamento de Quimica, Universidad de Los Andes, Carrera 1 No. 18A-12, Bogota 111711, Colombia. LA - eng PT - Journal Article DEP - 20221013 PL - Switzerland TA - Sensors (Basel) JT - Sensors (Basel, Switzerland) JID - 101204366 RN - 7782-42-5 (Graphite) RN - 7440-44-0 (Carbon) RN - 9012-76-4 (Chitosan) RN - 8NFQ3F76WR (morin) RN - 9IKM0I5T1E (Quercetin) RN - 0 (Flavonoids) RN - 5G06TVY3R7 (Rutin) SB - IM MH - Humans MH - *Graphite/chemistry MH - Carbon/chemistry MH - *Chitosan/chemistry MH - Quercetin MH - Electrodes MH - Flavonoids MH - Rutin PMC - PMC9608833 OTO - NOTNLM OT - chitosan OT - glassy carbon OT - graphene OT - morin OT - square wave voltammetry COIS- The authors declare no conflict of interest. EDAT- 2022/10/28 06:00 MHDA- 2022/10/29 06:00 PMCR- 2022/10/13 CRDT- 2022/10/27 01:55 PHST- 2022/09/10 00:00 [received] PHST- 2022/09/19 00:00 [revised] PHST- 2022/09/22 00:00 [accepted] PHST- 2022/10/27 01:55 [entrez] PHST- 2022/10/28 06:00 [pubmed] PHST- 2022/10/29 06:00 [medline] PHST- 2022/10/13 00:00 [pmc-release] AID - s22207780 [pii] AID - sensors-22-07780 [pii] AID - 10.3390/s22207780 [doi] PST - epublish SO - Sensors (Basel). 2022 Oct 13;22(20):7780. doi: 10.3390/s22207780.